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ALCOHOL L SCHOOL
DISTILLAT ATION AND MOLECULA AR SIEVES: A PRACTICAL VIEWPOINT
Cincinnati, Ohio U S A
Philip W.. Madson President
FUNDAM MENTALS O OF DISTILL LATION
TYPICAL DIISTILLATION RELATIO ONSHIPS CONDENSER
VAPOUR LOWER TEMPERATURE
COOLING WATER REFLUX LIQUID
FEED `
THERMAL ENERGY HIGHER TEMPERATURE
VAPOUR BOILING LIQUID
BOTTOMS PROD DUCT
OVERHEAD PRODUCT
TRAYS (CONTACTING DEVICES)
VAPOUR-LIQUID VAPOURD EQUILIBRIUM ETHANOL L-WATER
100 90 80 70 60
MOLE % ETHANOL IN VAPOUR
50 40 30 20 10 0 0
10
20
30
4 40
50
60
70
80
90
MOLE % ET THANOL IN LIQUID
100
100 90 80 70 60
MOLE % ETHANOL IN VAPOUR
50 40 30 20 10
(10 VOLUM ME % FEED)
0 0
10
20
30
4 40
50
60
70
80
90
MOLE % ET THANOL IN LIQUID
100
100 90 80 70 60
MOLE % ETHANOL IN VAPOUR
50 40 30 20 10
(10 VOLUM ME % FEED)
0 0
10
20
30
4 40
50
60
70
80
90
MOLE % ET THANOL IN LIQUID
100
100 90 80 70 60
MOLE % ETHANOL IN VAPOUR
50 40 30 20 10
(10 VOLUM ME % FEED)
0 0
10
20
30
4 40
50
60
70
80
90
MOLE % ET THANOL IN LIQUID
100
100 90 80 70 60
MOLE % ETHANOL IN VAPOUR
50 40 30 20 10
(10 VOLUM ME % FEED)
0 0
10
20
30
4 40
50
60
70
80
90
MOLE % ET THANOL IN LIQUID
100
100 90 80 70 60
MOLE % ETHANOL IN VAPOUR
50 40 30 20 10
(10 VOLUM ME % FEED)
0 0
10
20
30
4 40
50
60
70
80
90
MOLE % ET THANOL IN LIQUID
100
AZEOTROPE 194.4 PROOF 100 90 80 70 60
MOLE % ETHANOL IN VAPOUR
50 40 30 20 10
(10 VOLUM ME % FEED)
0 0
10
20
30
4 40
50
60
70
80
90
MOLE % ET THANOL IN LIQUID
100
AZEOTROPE 194.4 PROOF 100 90
EQUILIBRIUM CURVE
80 70 60
MOLE % ETHANOL IN VAPOUR
50 40 30 20 10
(10 VOLUM ME % FEED)
0 0
10
20
30
4 40
50
60
70
80
90
MOLE % ET THANOL IN LIQUID
100
STRUCTURING TH HE DISTILLATION SYSTEM STRATEGY S
STRIPPING SYST TEM
DEHYDRATION SYSTEM ANHYDROUS PRODUCT
RECTIFYING G SYSTEM 100 90
EQUILIBRIUM CURVE
AZEOTROPE 194.4 PROOF
80 70
MOLE % ETHANOL IN VAPOUR
SPIRIT
60 50 40 30 20 10
(10 VOLUME % FEED)
0
STILLAGE
0
10
20
30
40
50
60
70
80
90
100
MOLE % ETH HANOL IN LIQUID
OPERATIING LINE Locus of possible co oncentrations of liquid and vapour passing p in tower for a given energy inpu ut
StrippingStripping pp g-Co oncentrating g 14 lb STEAM per U.S S. GALLON (absolute) o or 1.7 Kg g STEAM M per LITER
ENE ERGY REQUIRE EMENTS ADVANCED-INTEGRATED
StrippingStripping pp g-Co oncentrating g 9 lb STEAM per U.S.. GALLON (absolute) o or 1.1 Kg g STEAM M per LITER
CONTACTIN NG DEVICES (TRA ( AYS))
DISTILLATION TR RAY FUNCTIONS • MIX RISING VAPOUR WITH FA ALLING LIQUID • ALLOW FOR SEPARATION AFT TER MIXING • PROVIDE PATH FOR LIQUID TO T PROCEED DOWN THE TOWER • PROVIDE PATH FOR VAPOUR TO PROCEED UP THE TOWER
ENRICHE ED VAPOUR LIQUID
V-L MIXING
STRIPPED LIQUID
VAPOUR
PERFORA ATED TRAYS OUTLET WEIR
DOWNCOMER AREA
INLET WEIR
DOWNCOMING LIQUID ENRICHED VAPOUR
V-L SEPARATION V-L MIXING
VAPOUR
STRIPPED LIQUID
PERFORATED TRAY T FROTHING OUTLET WEIR
IN NLET WEIR ENRICHED VAPOUR
DOWNCOMER AREA
DOWNCOMING LIQUID
FRO OTH ZONE
V-L SEPARATION
V-L MIXING
VAPOUR STRIPPED LIQUID
RELIAB BILITY BEER ST TRIPPER FOUL LING
DISC--DONU DISC UT TRAYS DON NUTS DESCENDING LIQUID DISC
DESCENDING LIQUID
ENRICHED VAPOUR
VAPOUR
STRIPPED STILLAGE
Bacardi Baca rdi
DISC--DONU DISC UT TRAYS DON NUTS DESCENDING LIQUID DISC
DESCENDING LIQUID
ENRICHED VAPOUR
FOULING
VAPOUR
STRIPPED STILLAGE
PERFORA ATED TRAYS OUTLET WEIR
INLET WEIR
DOWNCOMING LIQUID ENRICHED VAPOUR
DOWNCOMER AREA
FOULIN NG VAPOUR
STRIPPED LIQUID
BAFFLE - TRAY Y EXPERIENCE • 39 COMMERCIAL SYSTEMS S - SULFITE PULPING LIQUO OR - FERMENTED SULFITE LIIQUOR - FERMENTED LIGNOLIGNO IGNO-CEL CELLULOSE U OSE HYDROLYZATE HYDRO YZATE - FERMENTED WHOLE GR RAIN - ALCELL PULPING LIQUO OR - FERMENTED CHEESE WHEY W - FERMENTED CANE MOL LASSES
BAFFLE - TRAY Y EXPERIENCE • 5 YEAR CLEAN NING CYCLE FERMENTED GRAIN G • 1 YEAR CLEAN NING CYCLE FERMENTED CHEESE C WHEY • ELIMINATED ANTI A ANTI-FOAM AND ANTIANTISCALANT • 6-12 MONTH CLEANING C CYCLE FERMENTED “C” “ MOLASSES
