METHOD FINDER (Key on page MF 34]

M ETHO D FINDER (Ke y on p a g e M F! 34]

Chemical

M eth No.

M e th od Na m e

Flow Ra te ( L /m i n )

Vol. (L)

E x tr a c ti o n

A n a ly t ic a l T e c h n iq u e

Sampler

min max HPLC !FL/U V

P T F E & X A D !2

Acenaphthene

5506

PO LYN UC LEA R A RO M ATIC HYDR OC ARBO NS by H PLC

2.0

200 - 1000

ac eto nitr ile

Acenaphthene

5515

PO LYN UC LEA R A RO M ATIC HYDROCARBONS

2.0

200 - 1000

va r ies

Acenaphthylene

5506


2.0

200 - 1000

ac eto nitr ile

Acenaphthylene

5515


2.0

200 ! 1000

va r ies

A c e talde hyde

2018

ALIPHATIC ALDEHYDES

0.1 - 1.5

1 - 15

ACN

HP LC /UV

SG-DNPH

A c e talde hyde

2538

A C E T AL D E HY D E

0.01 - 0.05

1 ! 12

t ol

G C !F ID

X A D !2 /H M P

A c e talde hyde

2539

A L D EH Y D E S, SC R E E N IN G

0.01 - 0.05

5-5

t ol

G C !F ID /M S

X AD -2 /H M P

A c e talde hyde

3507


0.1 - 0.5

6 - 60

r ea g

HPLC !U V

BuB

Ac etic ac id

1603

AC ETIC AC ID

0.01 - 0.1

20 - 300

formic a

G C !FID

CCT

A c e tic anhydride

3506

A C E T IC A N H Y D R ID E

0.2 - 1.0

25 - 100

r ea g

VIS

BuB

Ac eto in

2558

AC ETO IN

0.01 - 0.2

1 - 10

Ac et-M eth

G C -FID

A -C M S

Acetone

1300

KETONES I

0.01 - 0.2

0.5 - 3

C S2

G C !FID

CCT

Acetone

2549

V O L A TI LE O R G A N IC C P D S (Screen in g)

0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Acetone

3800

ORG ANIC AND INORGAN IC GASES BY EXTR ACTIV E FTIR SPEC T R O MET R Y

0.1 - 2.0

Inst r. D ep .

NA

FTIR

Di r. R e a d

Acetone

2555

KETONES I

0.01 - 0.2

0.5 - 3.0

C S2

G C -FID

A -C M S

Ac eto ne cy an oh yd rin

2506

AC ETO NE CY AN O HY DR IN

0.2

0.3 - 12

Et Ac

G C !NPD

P or Q S

G C !FID HPLC !FL/U V G C !FID

P T F E & X A D !2 P T F E & X A D !2 P T F E & X A D !2

Ac eto nitr ile

1606

AC ETON ITRILE

0.01 - 0.2

1 - 25

M e C l/M e O H

G C !FID

CCT

A c e tyle ne dic hlor ide

1003

H Y D R O C A R B O N S , H A L O G E N A TE D

0.01 - 0.2

0.2 - 5

C S2

G C !FID

CCT

A c e tyle ne te trabr o m ide

2003

1,1,2,2 !T E TR A B R O M O E T H AN E

0.2 - 1.0

50 - 100

T HF

G C !FID

SG

A c e tyle ne te trac hlo r ide

1019

1,1,2,2 !T E TR A C H L O R O E TH A N E

0.01 - 0.2

3.0 - 30

C S2

G C !FID

PCT

-

2-

Ac ids , ino rg an ic

7903

AC IDS , INO RG AN IC

0.2 - 0.5

3.0 - 100

H C O 3 /C O 3

IC

SG(washed)

ACN

1606

AC ETON ITRILE

0.01 - 0.2

1 - 25

M e C l/M e O H

G C !FID

C C T lg

Ac ro lein

2501

AC RO LEIN

0.01 - 0.1

1.5 - 48

t ol

G C !NPD

X A D !2 /H M P

Ac ro lein

2539


0.01 - 0.05

5-5

t ol

G C !F ID /M S

X A D !2 /H M P

Ac rylo nitr ile

1604

AC RYLO NITRILE

0.01 - 0.2

3.5 - 20

a c et/C S 2

G C !FID

CCT

Ae ro bic ba cte ria

0801

A ER O BIC B AC TE RIA by G C -F AM E

28.3

50 - 300

hex/MTBE

G C -FID

i m p a c to r

Alach lor

5603

ALA C HLO R in AIR

1

70 - 1750

met h a nol

ELISA

SPE disk

A l ac hlo r

5602

CHLORINATED ORG ANONITROGEN H ER BIC ID ES (A IR SA M PL IN G )

0.2 - 1

12 - 480

reagent

G C /E C D

OV S-2

A l ac hlo r

9200

CHLORINATED ORG ANONITROGEN HER BICIDES (HAND WAS H)

NA

NA

NA

G C - EC D

polyethylene bag

A lac hlo r

9201

CHLORINATED ORG ANONITROGEN HE RBIC IDES (DER M AL P ATC H))

NA

NA

IPA/diazomethane

G C - EC D

PUF pad

Aldehydes, screening

2539


0.01 - 0.05

5-5

t ol

G C !F ID /M S

X A D !2

Aldicarb

5601

ORG ANONITROGEN PESTICIDES

0.1 - 1

var-480

reagent

HP LC - U V

OV S-2

Ald rin

5502

A L D R IN & L IN D A N E

0.2 - 1.0

18 - 240

isooct

G C !E C N

GFF & BuB

Alka line du sts

7401

ALKA LINE DU STS

1-4

70 - 1000

HCl

T it ra t ion

PTFE

A llyl alc oho l

1402

ALC O HO LS III

0.01 - 0.2

1 - 10

IP A/C S 2

G C !FID

CCT

A llyl alc oho l

1405

ALCOHO LS COM BINED

0.01 - 0.2

2 - 10

IP A -C S 2

G C -FID

CCT

A llyl c hlor ide

1000

A L LY L C H LO R I D E

0.01 - 1.0

16 - 100

bz

G C !FID

CCT

3/15/2003

MF!1

NIOSH Manual of Analytical Methods

Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Al lyl glyc idyl ethe r

2545

ALLYL GLYCIDYL ETHER

0.01 - 0.2

1.5 - 8

d ieth y l et h er

G C !FID

Tenax

A l lyl tric hlo r ide

1003

HYDROC ARBONS, HALOG ENATED

0.01 - 0.2

2 - 60

CS2

G C !FID

CCT

Alumina

0500

PARTICU LATES N.O.R .

1-2

7 - 133

!

Grav

P VC , ta re d

A l um inum

7300

E LE M E NT S b y IC P

1-4

5 - 100

H N O 3/HC lO 4

IC P !AES

MC EF

A l um inum

7303

E LE M EN TS by IC P (H O T B L O C K /H C l /H N O 3 D IG E S T IO N )

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

A l um inum

7301

ELE M EN TS b y IC P (A Q UA RE G IA A SH IN G )

1-4

5 - 100

H C l /H N O 3

ICP-AES

MC EF

A l um inum

7013

ALUMINUM & CPDS, as Al

1-3

10 - 400

HNO3

FAAS

MC EF

Am ine s, a liph atic

2010

AM INE S, A LIPH ATIC

0.01 - 1.0

3 - 30

H 2SO 4/a q M e O H

G C !FID

SG

Am ine s, a ro m atic

2002

AM INE S, A RO M ATIC

0.2 - 1.0

30 - 150

Et h a nol

G C !FID

SG

Aminobenzene

2002


0.2 - 1.0

30 - 150

Et h a nol

G C !FID

SG

Aminobenzene

2017

A N IL IN E , o - TO L U ID I NE , A N D N I TR O B E N Z EN E

0.2

5 - 50

Et h a nol

G C -FID

GFF + SG

2 !A m ino e thano l

2007

AMINOETHANO L COM POUNDS I

0.01 - 0.2

4 - 24

M eO H/H 2O

G C !FID

SG

2 !A m ino e thano l

3509

AM INO ETH AN O L C O M PO UN DS II

0.5 - 1.0

5 - 300

HSA

IC

IM P

2-aminotoluene

2017


0.2

5 - 50

et h a nol

G C -FID

GFF + SG

p !Am ino ph en yla rso nic ac id

5022

A R S E N IC , O R G A N O !

1-3

50 - 1000

b u ffer

IC !HYAAS

PTFE

2 !Aminotoluene

2002


0.02 - 1.0

10 - 150

Et h a nol

G C !FID

SG

Am m on ia

6015

AM M O NIA by VIS

0.1 - 0.2

0.1 - 90

H 2O

VIS !Au to

S G + H 2SO 4

Am m on ia

6016

AM M O NIA by IC

0.1 - 0.5

0.1 - 96

H 2O

IC

S G + H 2SO 4

n ! and s e c !Am yl ac etate

1450

ESTERS I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

n-Am yl ac etate

1450

ESTERS I

0.01 - 2

1 - 10

C S2

G C -FID

CCT

Am yl ac etate

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

iso-A my lace tate

1450

ESTERS I

0.01 - 2

1 - 10

C S2

G C -FID

CCT

Aniline

2002


0.02 - 0.2

5 - 30

Et h a nol

G C !FID

SG

Aniline

2017

ANILINE , O -TOLU IDINE, & N I TR O B E N Z EN E

0.2

5 - 50

et h a nol

G C -FID

GFF+SG

Aniline

8317

ANALINE an d @ -TOLUIDINE in urine

NA

NA

Alk

H P LC /E C D

NA

Anisidine

2514

A N IS ID I NE

0.5 - 1.0

24 - 320

MeOH

HPLC !U V

X A D !2

Anthracene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Anthracene

5515


2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

Antimony

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Antimony

7301


1-4

50 - 2000

H C l /H N O 3

ICP-AES

MC EF

p !Ar sa nilic ac id

5022

ARSENIC, organo!

1-3

50 - 1000

b u ffer

IC !HYAAS

PTFE

Ar se nic

7900

AR SENIC & compoun ds , a s As

1-3

30 - 1000

H N O 3/H 2SO 4/HC lO 4

HYAAS

MC EF

Ar se nic

7300


1-4

5 - 2000

H N O 3/HC lO 4

IC P !AES

MC EF

Ar se nic

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

Ar se nic

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Ar se nic

7301


1-4

5 - 2000

H C l /H N O 3

ICP-AES

MC EF

A r senic trio xide

7901

AR SENIC TR IOX IDE, as A s

1-3

30 - 1000

H N O 3/H 2O 2

G FAAS

MC EF

3/15/2003

MF!2


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Arsine

6001

A R S IN E

0.01 - 0.2

0.1 - 10

HNO3

G FAAS

CCT

A sbe sto s

7400

A S BE ST O S F IB ER S b y PC M

0.5 - 16

400 - va r

NA

PCM

MCEF open

A sbe sto s

7402

ASBESTOS FIBERS by TEM

0.5 - 16

400 - va r

NA

TEM

MCEF open

A sbe sto s

9000

ASBESTOS, CHRYSOTILE b y XR D

NA

NA

NA

XR D

bu lk

A sbe sto s

9002

ASBES TOS (bulk) by PLM

NA

NA

NA

PLM

bu lk

A sp arta m e

5031

A SP AR TA M E

1-3

70 - 1200

eluent

HPLC !U V

PTFE

A sp ha lt fu m e

5042

B E N Z EN E S O LU B LE F R AC T IO N A N D TOTAL PARTICULATE (ASPHALT FUME)

1-4

28 - 400

benzene

G RA VIM ETR IC

Tared PTFE

Atrazine

5602


0.2 - 1

12 - 480

reagent

G C /E C D

OV S-2

Atrazine

8315

TR IAZ INE HE RB IC IDE S a nd the ir METABOLITES

NA

NA

NA

GC-M SD

Urine

Atrazine

9200


NA

NA

NA

G C - EC D

polyethylene bag

Atrazine

9201


NA

NA

IP A/ diazomethane

G C - EC D

PUF pad

Az ela ic a cid

5019

AZ ELA IC A C ID

1-3

200 - 1000

Et h a nol

G C !FID

P VC

Azinphos methyl

5600

ORG ANOPHO SPHORUS PESTICIDES

0.2 - 1.0

12 - 240

t ol/a cet

G C !FPD

O VS !2

Ba cte ria

0801

A ER O BIC B AC TE RIA by G C -F AM E

28.3

50 - 300

hex/MTBE

G C -FID

i m p a c to r

B[a]P

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

B[a]P

5515


2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

Bar ium

7056

B A R IU M , S O LU B LE C O M P O U N D S

1-4

50 - 2000

H 2O

FAAS

MC EF

Bar ium

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

Bar ium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Bar ium

7301


1-4

50 - 2000

H C l /H N O 3

ICP-AES

MC EF

Benomyl

5601


0.1 - 1

var - 480

reagent

HP LC - U V

OV S-2

Be nzalde hyde

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Benz[a]anthracene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Benz(a)anthracene

5515


2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

Benzene

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Benzene

3700

B EN ZE NE by po rta ble G C

> 0.02

80% vol

NA

GC

air bag

Benzene

1501

HY DR O C AR BO NS , AR O M ATIC

0.01 - 0.2

5 - 30

C S2

G C !FID

CCT

Benzene

1500

HYDROC ARBONS, BP 36 !216 °C

0.01 - 0.2

2 - 30

C S2

G C !FID

CCT

Benzene

3800

ORG ANIC and INORGANIC G ASES by EX TR ACTIV E FTIR SPE C T R O MET R Y

0.1 - 2.0

Inst r. D ep .

NA

FTIR

Di r. R e a d

Be nzene so lubles

5042


1-4

28

benzene

Grav

Tared PTFE

1, 3-be nze ne diol

5701

R ES O RC IN O L

0.2 - 1

5 - 160

met h a nol

G C -FID

OV S-7

Be nzidine D ye s

5013

DYES

1-3

150 - 500

H 2O

HPLC !U V

PTFE

Benzidine

5509

BENZIDINE and 3,3'!DICHLORO !B E N Z ID I NE

0.2

20 - 100

triethyl amine /M e O H

HPLC !U V

GFF

Benzo[a]pyrene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Benzo(a)pyrene

5515


2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

3/15/2003

MF!3


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Benzo[a]fluoranthene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Benzo(b)fluoranthene

5515


2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

Benzo[e]pyrene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Benzo(e)pyrene

5515


2.0

200 - 1000

va r ies

G C !ID

P T F E & X A D !2

Benzo[k]fluoranthene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Benzo(k)fluoranthene

5515


2.0

200 - 1000

va r ies

G C !ID

P T F E & X A D !2

Benzo[ghi]perylene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Benzo(ghi)perylene

5515


2.0

200 - 1000

va r ies

G C !ID

P T F E & X A D !2

Be nzo su lfon az ole

2550

B EN ZO TH IA ZO LE IN AS PH A LT F UM E

1.0 - 2.0

480 - 960

hexane

G C - SC D

PTFE + X D-2

Be nzo thia zo le

2550


1.0 - 2.0

480 - 960

hexane

G C - SC D

PTFE + X D-2

Be nzoyl pe r o xide

5009

B E N Z O Y L P E R O X ID E

1-3

40 - 400

d ieth y l et h er

HPLC !U V

MC EF

Be nzyl c hlo ride

1003


0.01 - 0.2

6 - 50

C S2

G C !FID

CCT

Be r yllium

7300


1- 4

1250-2000

H N O 3/HC lO 4

IC P !AES

MC EF

Be r yllium

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

Be r yllium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Be r yllium

7301


1-4

1250-2000

H C l /H N O 3

ICP-AES

MC EF

Be r yllium & c o m po und s

7102

BERYLLIUM and cpds, as Be

1-4

25 - 2000

H N O 3/H 2SO 4

G FAAS

MC EF

Bio ae r o so l

0800

BIOA ERO SO L SAM PLING (Indoor A ir)

28.3

va r ies

NA

va r ies

I m p a c to r

Biphenyl

2530

DIPHENYL

0.01 - 0.5

15 - 30

C C l4

G C !FID

Te na x G C

Bism uth

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

B itu m en fu m e

5042


1-4

28 - 400

benzene

Grav

Tared PTFE

Bo r o n

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Bo r o n c ar bide

7506

B O R O N C A R B ID E

1.7 or 2 .2

100 - 1000

ash

XR D

C Y C & P VC

Bo r o n o xide

0500


1.5 - 2.0

25 - 133

NA

Grav

P VC

Brom oform

1003


0.01 - 0.2

4 - 70

C S2

G C -FID

CCT

Bromine

6011

C H L O R IN E a n d B R O M I N E

0.3 - 1.0

8 - 360

N a 2S 2O 3

IC

Ag F

1-Bromopropane 2-Bromopropane

1025

1 - a n d 2 -B R O M O P R O P A N E

0.01 - 0.2

0.1 - 12

C S2

G C -FID

CCT

Brom oform

1003


0.01 - 0.2

4 - 70

C S2

G C !FID

CCT

Bromotrifluoromethane

1017

T R IF L UO R O B R O M O M E T HA N E

0.01 - 0.05

0.3 - 1.0

C H 2C l2

G C !FID

2 C C T (lg + sm )

Bro m ox yn il

5010

BRO MO XYN IL and B 'OC TANO ATE

1-3

2 - 400

C H 3C N

HPLC !U V

PTFE

Brom oxy nil octa noa te

5010


1-3

90 - 400

C H 3C N

HPLC !U V

PTFE

1,3 !Butadiene

1024

1,3 !B U TA D IE N E

0.01 - 0.5

5 - 25

C H 2C l2

G C !FID

CCT

2 !Butanone

2500

M E T H YL E TH Y L K E TO N E

0.01 - 0.2

1 - 12

C S2

G C !FID

C a rb o n b e a d s

2 !Butanone

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

2-Butanone

3800


0.1 - 2.0

Inst r. D ep .

NA

FTIR

Di r. R e a d

3/15/2003

MF!4


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Bu tox ya ce tic a cid

8316

BUTOXYACETIC ACID in urine

NA

NA

NA

G C - EC D

NA

2 !Buto xye thyano l

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

2 !Buto xye thano l

1403

ALC O HO LS IV

0.01 - 0.05

2 - 10

C H 2C l2/M e O H

G C !FID

CCT

n !, s ec !, & t!Buty l ace tate

1450

ESTERS I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

Buty l ace tate

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

iso-Bu tyl ac etate

1450

ESTERS I

0.01 - 2

1 - 10

C S2

G C -FID

CCT

1-Bu tyl ac etate

1450

ESTERS I

0.01 - 2

1 - 10

C S2

G C -FID

CCT

Butyl alc o ho l

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

tert !Butyl alc o ho l

1400

ALCOHO LS I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

n ! & s e c !Butyl alc o hol

1401

ALC O HO LS II

0.01 - 0.2

2 - 10

C S2

G C !FID

CCT

n- Butyl alc oho l

1405

ALCOHO LS COM BINED

0.01 - 0.2

2 - 10

IP A -C S 2

G C -FID

CCT

se c -Butyl alc o ho l

1405

ALCOHO LS COM BINED

0.01 - 0.2

2 - 10

IP A -C S 2

G C -FID

CCT

n !Butylamine

2012

n !B U TY L AM I N E

0.01 - 1.0

2 - 100

MeOH

G C !FID

S G + H 2SO 4

Butyl cellosolve

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Butyl cellosolve

1403

ALC O HO LS IV

0.01 - 0.05

1 - 10

C H 2C l2/M e O H

G C !FID

CCT

1,3 !Butyle ne glygo l

5523

GLYC OLS

0.5 - 2

5 - 60

MeOH

G C !FID

O VS !7

Butyl glyc idyl e the r

1616

BUTYL GLYCIDYL ETHER

0.01 - 0.2

15 - 30

C S2

G C !FID

CCT

n !Butyl me rc aptan

2525

n !BU TYL MER CAPTAN

0.01 - 0.05

1-4

a cet

G C !FPD

Chrom 104

n !Butyl me rc aptan

2542

M E R C A P TA N S

0.1 - 0.2

10 - 150

H C l/D C E

G C !FPD

GFF/HgAc

p !tert !Butyltoluene

1501


0.01 - 0.2

1 - 29

C S2

G C !FID

CCT

Butyr alde hyde

2539


0.05

5-5

t ol

G C !F ID /M S

X A D !2 /H M P

C a dm ium

7300


1-4

13 - 2000

H N O 3/HC lO 4

IC P !AES

MC EF

C a dm ium

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

C a dm ium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

C a dm ium

7301


1-4

13 - 2000

H C l /H N O 3

ICP-AES

MC EF

C a dm ium & c o m po un ds

7048

C A D M IU M a nd c pd s, as C d

1-3

25 - 1500

H N O 3/H C l

FAAS

MC EF

C a lc ium

7300


1-4

5 - 200

H N O 3/HC lO 4

IC P !AES

MC EF

C a lc ium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

C a lc ium

7301


1-4

5 - 200

H C l /H N O 3

ICP-AES

MC EF

C a lc ium & c o m po und s

7020

C A LC IU M a nd c pd s a s C a

1-3

20 - 400

H N O 3/HC lO 4

FAAS

MC EF

C a m pho r

1301

KE TO NE S II

0.01 - 0.2

1 - 25

M e O H /C S 2

G C !FID

CCT

C a m pho r

2553

KE TO NE S II

0.01 - 0.2

1 - 25

IP A -C S 2

G C -FID

A -C M S

C ap sa icin

5041

C AP SA ICIN an d D IHY DR O C AP SA ICIN

1-3

5 - 1000

C H 3C N

HPLC !FL

GFF

C a ptan

5601


0.1 - 1

var-480

reagent

HP LC - UV

OV S-2

C a ptan

9205

CAPTAN and THIOPHENATE-METHYL o n D E RM A L P A TC H

NA

NA

IP A /A C N

HP LC - U V

Patch

C a ptan

9202

CAPTAN and THIOPHENATE-METHYL in Handrinse

NA

NA

NA

HP LC - U V

Hand wa sh

Carbaryl

5601


0.1 - 1

var-480

reagent

HP LC - UV

OV S-2

Carbaryl (Sevin)

5006

CARBARYL

1-3

20 - 400

reagent

VIS

GFF

3/15/2003

MF!5


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max C ar be nd az im

5601


0.1 - 1

var - 480

reagent

HP LC - U V

OV S-2

C a r bito l

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

C a r bo fur an

5601


0.1 - 1

var-480

reagent

HP LC - U V

OV S-2

C a r bo n blac k

5000

C A R BO N B LA C K

1-2

30 - 570

NA

Grav

P VC

C a r bo n, e le m e ntal

5040

ELEM ENTA L CA RBO N (DIES EL PA RT.)

2-4

142-19000

t h erma l

E G A/TO A

QFF

C a r bo n dio xide

6603

C A R B O N D IO X I D E

0.02 - 0.1

80% vol

NA

G C !T C D

air bag

C a r bo n disulfide

1600

C A R B O N D IS U LF ID E

0.01 -0 .2

2 - 25

toluene

G C !FPD

CC T & d ry tu b e

C a r bo n m o no xide

6604

CARBON MONOXIDE

NA

NA

NA

Sens or

Port In str

C a r bo n te trac hlo r ide

1003


0.01 - 0.2

3 - 150

C S2

G C !FID

CCT

* -3-Carene

1552

TERPENES

0.01 - 0.02

2 - 30

C S2

G C !FID

CCT

Cellulose

7404

C E LL UL OS E IN SU LA TIO N

1

NA

NA

SEM

ACF

Chlordane

5510

CHLORDANE

0.5 - 1.0

10 - 200

t ol

G C !E C D

M C E F & Ch ro m 102

Chlorinated camphene

5039

C H L O R IN A T ED C A M P H E N E

0.2 - 1

2 - 30

p et eth er

G C !E C D

MC EF

C hlo rinate d diphe nyl ox ide

5025

C H L O R IN A T ED D IP H E N YL O X ID E

0.5 - 1.5

8 - 200

isooctane

G C !E C N

MC EF

Chlorinated terphenyl

5014

CH LORINA TED TERPH ENYL

1-3

100 - 1500

isooctane

G C !E C D

GFF

Chlorine

6011


0.3 - 1.0

2 - 90

N a 2S 2O 3

IC

Ag F

C hlo ro ac e talde hyde

2015

C H L O R O A C E T AL D E HY D E

0.05 - 0.2

3 - 16

MeOH

G C !E C D

SG

C hlo ro ac etic ac id

2008

C HLO RO AC ETIC AC ID

0.05 - 0.2

1 - 100

H 2O

IC

SG

Chlorobenzene

1003


0.01 - 0.2

1.5 - 40

C S2

G C !FID

CCT

p -Chlo r o be nzo tr ifluo r id e

1026

p - C H LO R O B E N Z O T RI FL U O R ID E

0.01 - 0.2

0.1 - 10

C S 2/M e O H

G C -FID

CCT

Chlorobromomethane

1003


0.01 - 0.2

0.5 - 60

C S2

G C -FID

CCT

Chlorobromomethane

1003


0.01 - 0.2

0.5 - 8

C S2

G C !FID

CCT

Chlorodifluoromethane

1018

D I C H LO R O D I F LU O R O M E T H A N E

0.01 - 0.05

1-4

C H 2C l2

G C !FID

2 C C T (lg + sm )

Chlorodiphenyl (42 & 54% C I)

5503

POLY CH LORO BIPHENY LS

0.05 - 0.2

1 - 50

hexane

G C !E C D

G FF & F lor isil

2 !Chlo ro e thano l

2513

ETH YLE NE CH LO RO HY DR IN

0.01 - 0.2

2 - 35

IP A /C S 2

G C !FID

PCT

Ch loroform

1003


0.01 - 0.2

1 - 50

C S2

G C !FID

CCT

4 !Chloronitrobenzene

2005

N I TR O A R O M A T IC C O M P O U N D S

0.01 - 1.0

1 - 150

MeOH

G C !FID

SG

p !Chlo ro phe no l

2014

p !C H L O RO P H EN O L

0.05 - 0.2

1.5 - 40

C H 3C N

HPLC !U V

SG

Chloroprene

1002

$!C H L O R O P R E N E

0.01 - 0.1

1.5 - 8

C S2

G C !FID

CCT

C hlo rpr o pham

5601


0.1 - 1

var-480

reagent

HP LC , U V

OV S-2

C hlo rpyr ifo s

5600


0.2 - 1.0

12 - 240

t ol/a cet

G C !FPD

O VS !2

C hr om ic a cid

7600

C H R O M I U M , HE X A V A LE N T

1-4

8 - 400

reagent

VIS

P VC

C hr om ic a cid

7604


1-4

100 - 1000

N a O H / N a2 C O 3

IC

P VC

C hr o m ium

7024

C H R O M IU M a nd c pd s, as C r

1-3

10 - 1000

H C l /H N O 3

FAAS

MC EF

C hr o m ium

7300


1-4

5 - 1000

H N O 3/HC lO 4

IC P !AES

MC EF

C hr o m ium

7301


1-4

5 - 1000

H C l /H N O 3

ICP-AES

MC EF

C hr o m ium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

C hr o m ium

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

Chromium, hexavalent

7600


1-4

8 - 400

reagent

VIS

P VC


7604


1-4

100 - 1000


IC

P VC

3/15/2003

MF!6


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Chromium, hexavalent

7605

C H RO M IU M HE XA VA LE NT b y IO N CHROM ATOGRAPHY

0.1 - 4

1 - 400

N a O H - N a2C O 3

IC

P VC


7703

CHROM IUM, HEXAV ALENT b y Field Portab le Spe ctroph otom etry

1-4

10 - 1200

( N H4) 2SO 4/ N H4O H

VIS

PVC, MCE, PTFE


9101

CHROM IUM, HEXAV ALENT in s ett led dust

NA

NA

NA

Sp ot

Te st s trip

Chrysene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Chrysene

5515

PO LYN UC LEA R A RO M ATIC HYDROC ARBONS

2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

C oal tar naphtha

1550

NAPHTHAS

0.01 - 0.2

1.3 - 20

C S2

G C !FID

CCT

C oal tar pitc h vo latile s

5042


1-4

28 - 400

benzene

Grav

tared PTFE

C ob alt

7300


1-4

25 - 2000

H N O 3/HC lO 4

IC P !AES

MC EF

C ob alt

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

C ob alt

7301


1-4

25 - 2000

H C l /H N O 3

ICP-AES

MC EF

C ob alt

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

C obalt & c o m po unds

7027

C O B A LT an d c p ds , a s C o

1-3

30 - 1500

a q re g /H N O 3

FAAS

MC EF

C oppe r

7300


1-4

5 - 1000

H N O 3/HC lO 4

IC P !AES

MC EF

Co ppe r

7301


1-4

5 - 1000

H C l /H N O 3

ICP-AES

MC EF

Co ppe r

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

Co ppe r

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Co ppe r (dust & fum e )

7029

CO PPER (dust & fumes)

1-3

50 - 1500

H N O 3/H C l

FAAS

MC EF

Cr e so l

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Cre sol, all isome rs

2546

C R ES O LS an d P HE NO L

0.01 - 0.1

1 - 24

MeOH

G C !FID

X A D !7

Cr o tonalde hyde

2539


0.01 - 0.05

5-5

t ol

G C !F ID /M S

X A D !2 /H M P

Cr o tonalde hyde

3516

C R O T O N A L D EH Y D E

0.1 - 0.2

1 - 49

b u ffer

DPP

BuB

Cryofluorane

1018

DICHLORODIFLUORO METHANE, 1,2 !DICHLOROTETR AFLU O R O ! ETHA NE, & C H L O R O D IF L UO R O M E T H A N E

0.01 - 0.05

1-4

C H 2C l2

G C !FID

2 CCT

Cum ene

1501


0.01 - 0.2

1 - 30

C S2

G C !FID

CCT

Cyanides

7904

CYANIDES, aerosol an d g a s

0.5 - 1.0

10 - 180

KOH

ISE

MCEF & BuB

Cyanides

6010

H Y D R O G E N C Y A N ID E

0.05 - 0.2

0.6 - 90

H 2O

VIS

s od a lim e

C ya nu ric ac id

5030

C YA NU RIC AC ID

1-3

10 - 1000

rea ge nts

HPLC !U V

P VC

Cyanazine

5602


0.2 - 1

12 - 480

reagent

G C /E C D

OV S-2

Cyanazine

8315


NA

NA

NA

GS-MSD

Urine

Cyanazine

9200


NA

NA

NA

G C - EC D

polyethylene bag

Cyanazine

9201


NA

NA

IPA/diazomethane

G C - EC D

PUF pad

Cyclohexane

1500


0.01 - 0.2

2.5 - 5

C S2

G C !FID

CCT

Cyc lo he xano l

1402

ALC O HO LS III

0.01 - 0.2

1 - 10

IP A /C S 2

C G !FID

CCT

Cyc lo he xano l

1405

ALCOHO LS COM BINED

0.01 - 0.2

2 - 10

IP A -C S 2

G C -FID

CCT

3/15/2003

MF!7


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Cyclohexanone

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Cyclohexanone

2555

KETONES I

0.01 - 0.2

1 - 10

C S2

G C -FID

A -C M S

Cyclohexanone

1300

KETONES I

0.01 - 0.2

1 - 10

C S2

C G !FID

CCT

Cyclohexene

1500


0.01 - 0.2

5-7

C S2

C G !FID

CCT

1,3 !Cyclopentadiene

2523

1,3 !C Y C L O P E N TA D IE N E

0.01 - 0.05

1-5

Et Ac

G C !FID

Chrom104/ maleic anhy

2,4 !D

5001

2,4 !D an d 2,4,5 !T

1-3

15 - 200

MeOH

HPLC !U V

GFF

2,4-D a cid; 2,4-D,2 -ethylhe xyl ester; 2, 4-D , 2-buto xye thyl ester

5602


0.2 - 1

12 - 480

reagent

G C - EC D

OV S-2


9200


NA

NA

NA

G C - EC D

polyethylene bag


9201


NA

NA

IPA/diazomethane

G C - EC D

PUF pad

D ec abr o mo diphe nyl Ox i de

2559

D E C A B R O M O D I PH E N Y L O X I D E

2.0

48 - 960

T ol

G C /N C D

GFF

n !Decane

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

n-Decane

1500

o HYDROC ARBONS, BP 36 o-216 C

NA

NA

C S2

G C -FID

CCT

D eme to n

5514

D EM E TO N

0.2 - 1.0

30 - 500

toluene

G C !FPD

M CE F & X A D !2

Desethylatrazine

8315


NA

NA

NA

GC-M SD

Urine

Desisopropylatrazine

8315


NA

NA

NA

GC-M SD

Urine

D i ac eto ne alc oho l

1402

ALC O HO LS III

0.01 - 0.2

1 - 10

IP A /C S 2

G C !FID

CCT

D i ac eto ne alc oho l

1405

ALCOHO LS COM BINED

0.01 - 0.2

1 - 10

IP A -C S 2

G C -FID

CCT

Diacetyl

2557

DIACETYL

0.01 - 0.2

1 - 10

Ac et-M eth

G C -FID

A -C M S

o !Dianisidine

5013

DYES

1-3

150 - 500

H 2O

HPLC !U V

PTFE

Diato ma ce ou s ea rth

7501

SILICA, AMOR PHOUS

1-3

50 - 400

ash

XR D

PVC/CYC

D i azino n

5600


0.2 - 1

12 - 240

toluene/acetone

G C !FPD

O VS !2

Diazomethane

2515

D I AZ O M E T H A N E

0.2

6 - 30

C S2

G C !FID

X A D !2 ( c o at e d )

Dibenz[a,h]anthracene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Dibenz(a,h) anthracene

5515


2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

Diborane

6006

D I BO R A N E

0.5 - 1.0

60 - 260

H 2O 2

PES

P TF E & C C T w / o xi d iz e r

Dibromodifluoromethane

1012

D I FL U O R O D IB R O M O M E T H A N E

0.01 - 0.2

2.5 - 10

IPA

G C !FID

2 CCT

2 !D ibutylam ino e thanol

2007

A M I N O E TH A N O L C O M P O U N D S

0.01 - 0.2

4 - 24

M eO H/H 2O

G C !FID

SG

Dibu tyl ph osp ha te

5017

DIBUTY L PHO SPH ATE

1-3

50 - 250

C H 3C N

G C !FPD

PTFE

Dibu tyl ph tha late

5020

D I BU T YL P HT H A LA T E & DI(2 !ETHY LHEX YL) PHTH ALATE

1-3

6 - 200

C S2

G C !FID

MC EF

Dibutyltin bis(isooctyl m e r c apto ac e tate )

5504

O R G A N O T IN C O M P O U N D S

1 - 1.5

50 - 500

A c etic a /C H 3C N

HP LC /G FAAS

G F F + X A D !2

o !, p !Dichlorobenzene

2549


0.01 - 0.05

1-6

va r ies

TD /G C !M S

TD

o-Dichlorobenzene

1003


0.01 - 0.2

1 - 10

C S2

G C -FID

CCT

3/15/2003

MF!8


Chemical

M eth No.


M e th od Na m e

Vol. (L)

E x tr a c ti o n


Sampler

min max p-Dichlorobenzene

1003


0.01 - 0.2

1-8

C S2

G C -FID

CCT

p !Dichlorobenzene

1003


0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

3,3'!Dichlorobenzidine

5509

BENZIDINE an d 3,3'!D I C H LO R O B E N Z ID I NE

0.2

20 - 100

TE A/M e O H

HPLC !U V

GFF

Dichlorodifluoromethane

1018

DICHLORODIFLUORO METHANE, 1,2 !DICHLOROTETR AFLUO R O ! ETHANE & C H L O R O D IF L UO R O M E T H A N E

0.01 - 0.05

1-4

C H 2C l2

G C !FID

2 CCT (lg + sm )

1,1 !Dichloroethane

1003


0.01 - 0.2

0.5 - 15

C S2

G C !FID

CCT

1,2 !Dichloroethane

1003


0.01 - 0.2

0.5 - 50

C S2

G C !FID

CCT

D i c hlo r o e thyl e the r

1004

DICHLOROETHYL ETHER

0.01 - 1.0

2 - 15

C S2

G C !FID

CCT

1,2 !Dichloroethylene

1003


0.01 - 0.2

0.2 - 5

C S2

G C !FID

CCT

Dichlorofluoromethane

2516

D I C H LO R O F L U O R O M E T HA N E

0.01 - 0.05

0.25 - 3

C S2

G C !FID

2 C CT ( lg )

Dichloromethane

1005

M E T H YL E N E C H L O R ID E

0.01 - 0.2

0.5 - 2.5

C S2

G C !FID

2 CCT

Dichloromethane

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

1,1 !Dichlo ro !1 !nitroethane

1601

1,1 !DICHLORO !1 !N I TR O E T H AN E

0.01 - 1.0

1.5 - 15

C S2

G C !FID

PCT

1,2 !Dichloropropane

1013

P R O P Y LE N E D IC H L O R ID E

0.01 - 0.2

0.1 - 3.5

Acet/cyclohexane

G C !E C N

PCT

1,2 !D ic hlo r o te trafluoroethane

1018

DIC HLO RO DIFLUO RO ME THAN E, 1,2 !DICHLOROTETR AFLUO R O ! ETHANE & C H L O R O D IF L UO R O M E T H A N E

0.01 - 0.05

1-4

C H 2C l2

G C !FID

2 CCT (lg + sm )

D i c ro to pho s

5600


0.2 - 1

12 - 240

t ol/a cet

G C !FPD

O VS !2

Diesel exhaust

5040


1-4

142 -19000

t h erma l

E G A/TO A

QFF

Diethanolamine

3509


0.5 - 1.0

5 - 300

HSA

IC

IM P

Diethylamine

2010


0.01 - 1.0

3 - 30

H 2SO 4/M e O H

G C !FID

SG

2 !D ie thylam ino e thanol

2007


0.01 - 0.2

4 - 24

M eO H/H 2O

G C !FID

SG

D i e thyle ne glyc o l

5523

GLYC OLS

0.5 - 2

5 - 60

MeOH

G C !FID

O VS !7

D i e thyle ne glyc o l e ther

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Diethylenetriamine

2540

ETHYLENEDIAMINE, DIETHY LENE TRIAM INE, & T R IE T HY L EN E TE T RA M I N E

0.01 - 0.1

1 - 20

DMF

HPLC !U V

X A D !2 w/10 % N ITC

D i!(2 !ethy lhexy l) phth alate

5020

DIBUTYL PHTHALATE an d DI(2 !ETHY LHEX YL) PHTH ALATE

1-3

10 - 200

C S2

G C !FID

MC EF

Difluorodibromom ethane

1012


0.01 - 0.2

2.5 - 10

IPA

G C !FID

2 CCT

Difluorodichloromethane

1018

DIC HLO RO DIFLUO RO ME THAN E, 1,2 !DICHLOROTETR AFLU O R O !ET HAN E & C H L O R O D IF L UO R O M E T H A N E

0.01 - 0.05

1-4

C H 2C l2

G C !FID

2 CCT

Dih yd ro ca ps aic in

5041


1-3

7 - 1000

C H 3C N

HPLC !FL

GFF

Diisobutyl ketone

1300

KETONES I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

Diisobutyl ketone

2555

KETONES I

0.01 - 0.2

1 - 10

C S2

G C -FID

A -C M S

D i m e thylac e tam ide

2004

DIMETHYLACETAMIDE and D I M E TH Y L FO R M A M I D E

0.01 - 1.0

15 - 80

MeOH

G C !FID

SG

Dimethylamine

2010


0.01 - 1.0

3 - 30

H 2SO 4/M e O H

G C !FID

SG

2-(D im e thylam ino )e thanol 1-D im e thylam ino -2-propan ol

2561

2 -(D IM E TH YL AM IN O )E TH A NO L 1 -D IM E TH YL AM IN O -2 -P RO P AN O L

0.02 - 0.1

10 - 24

MeOH

G C -FID

XAD

N,N !Dimethylaniline

2002


0.02 - 1.0

3 - 30

Et h a nol

G C !FID

SG

Dim eth yla rsin ic a cid

5022


1-3

50 - 1000

b u ffer

IC !HYAAS

PTFE

3/15/2003

MF!9


Chemical

M eth No.


M e th od Na m e

Vol. (L)

E x tr a c ti o n


Sampler

min max Dim e thylfo rmamide

2004

DIMETHYLACETAMIDE & D I M E TH Y L FO R M A M I D E

0.01 - 1.0

15 - 80

MeOH

G C !FID

SG

1,1 !Dimethylhydrazine

3515

1,1 !D I M E TH Y L HY D R A Z IN E

0.2 - 1.0

2 - 100

reagent

VIS

BuB (0.1 M HC l)

N,N !Dimethyl!p !toluidine

2002


0.02 - 1.0

20 - 100

Et h a nol

G C !FID

SG

Dim ethy l sulfate

2524

DIM ETHY L SULFA TE

0.01 - 0.2

0.25 - 12

d iEt eth er

G C !E C N

Por P

Dioxane

1602

D I O X AN E

0.01 - 0.2

0.5 - 15

C S2

G C !FID

CCT

Diphenyl

2530

DIPHENYL

0.01 - 0.5

15 - 30

C C l4

G C !FID

Te na x G C

D i pro pyle ne glyc o l mo no m e thyl e the r

2554

GLYCOL ETHER S

0.1 - 0.2

3 - 25

M e C l2/Me th

G C -FID

A-747

D i sulfo to n

5600


0.2 - 1

12 - 240

t ol/a cet

G C !FPD

O VS !2

D i uro n

5601


0.1 - 1

var-480

reagent

HP LC , U V

OV S-2

o

o

n-Dodecane

1500

HYDROC ARBONS, BP 36 -216 C

NA

NA

C S2

G C -FID

CCT

D y e s ! benzidine !, o !tolidine !, o !dianisidine !

5013

D Y E S , B E N ZI D IN E !, o ! T O LI D IN E !, o ! D IA N IS ID I NE

1-3

150 - 500

H 2O

HPLC !U V

PTFE

E le me ntal c ar bo n

5040


2-4

142 -19000

t h erma l

E G A-TO A

QFF

Elem ents

7300


1-4

V a r ies

H N O 3/HC lO 4

IC P !AES

MC EF

Elem ents

7301

ELEMENTS by ICP (Aqu a R eg ion Ashin g)

1-4

V a r ies

Aq R eg

ICP-AES

MC EF PVCF

Elem ents

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

En dr in

5519

EN DR IN

0.5 - 1.0

12 - 400

t ol

G C !E C D

MCEF & Chrom 102

Ep ich lor oh yd rin

1010

EP ICH LO RO HY DR IN

0.01 - 0.2

2 - 30

C S2

G C !FID

CCT

EPN

5012

EPN

1-2

15 - 700

isooctane

G C !FPD

GFF

1,2 !Epoxypropane

1612

P R O P Y LE N E O X ID E

0.01 - 0.2

0.5 - 5

C S2

G C !FID

CCT

$ -Estradiol

5044

E S TR O G E N I C C O M P O U N D S

1

150 - 1000

M eth

HP LC - U V

PTFE

Estrone

5044


1

150 - 1000

M eth

HP LC - U V

PTFE

$ -Estro diol-3 -Ben zoa te

5044


1

150 - 1000

M eth

HP LC - U V

PTFE

E thano l

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

E thano l

1400

ALCOHO LS I

0.01 - 0.05

0.1 - 1

2 -b u ta n ol/C S 2

G C !FID

CCT

Ethanolamine

2007


0.01 - 0.2

4 - 24

5600

G C !FID

SG

E thio n

5600


0.2 - 1

12 - 240

t ol/a cet

G C !FPD

O VS !2

E tho pr o p

5600


0.2 - 1

12 - 240

t ol/a cet

G C !FPD

O VS !2

2 !Etho xye thano l

1403

ALC O HO LS IV

0.01 - 0.05

1-6

MeOH

G C !FID

CCT

2 !Etho xye thyl a ce tate

1450

ESTERS I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

Ethy l ace tate

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Ethy l ace tate

1457

ETHY L AC ETATE

0.01 - 0.2

0.1 - 10

C S2

G C !FID

CCT

Ethy l acry late

1450

ESTERS I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

Ethyl amyl ketone

1301

KE TO NE S II

0.01 - 0.2

1 - 25

M e O H /C S 2

G C !FID

CCT

Ethylbenzene

1501


0.01 - 0.2

1 - 24

C S2

G C !FID

CCT

E thyl bro m ide

1011

E T HY L BR O M I D E

0.01 - 0.2

0.5 - 4

IPA

G C !FID

CCT

Ethyl butyl ketone

1301

KE TO NE S II

0.01 - 0.2

1 - 25

M e O H /C S 2

G C !FID

CCT

E thyl c hlo ride

2519

E T HY L C H LO R I D E

0.02 - 0.05

0.3 - 3

C S2

G C !FID

2 CC T ( lg )

Eth yle ne ch lor oh yd rin

2513


0.01 - 0.2

2 - 35

IP A /C S 2

G C !FID

PCT

3/15/2003

MF!10


Chemical

M eth No.


M e th od Na m e

Vol. (L)

E x tr a c ti o n


Sampler

min max Ethylenediamine

2540

ETHY LENE DIAM INE, DIETHY LENE TRIAM INE, & T R IE T HY L EN E TE T RA M I N E

0.01 - 0.1

1 - 20

DMF

HPLC !U V

X A D !2 w/10 % N ITC

E thyle ne dibr o m ide

1008

E T HY L EN E D IB R O M I D E

0.02 - 0.2

0.1 - 25

b z/M e O H

G C !E C D

CCT

E thyle ne dic hlor ide

1003


0.01 - 0.2

1 - 50

C S2

G C !FID

CCT

E thyle ne glyc o l

5523

GLYC OLS

0.5 - 2

5 - 60

MeOH

G C !FID

O VS !7

Ethy lene glyc ol dinitra te

2507

N ITR O G LY C ER IN & ETH YL EN E G LY C O L DINITRA TE

0.2 - 1.0

3 - 100

Et h a nol

G C !E C D

Te na x G C

E thyle ne o xide

1614

E T HY L EN E O X ID E

0.05 - 0.15

1 - 24

DMF

G C !E C D

PC T w/HB r

E thyle ne o xide

3702

E TH YL EN E O X ID E b y p orta ble G C

> 0.02

80% vol

NA

G C !PID

air bag

E thyle ne o xide

3800


0.1 - 2.0

Inst r. d ep .

NA

FTIR

Di r. R e a d

E thyle ne thio ur e a

5011

ETHYLENE THIOUREA

1-3

200 - 800

H 2O

VIS

PVC or MCEF

Ethylenimine

3514

E T HY L EN I M IN E

0.2

1 - 48

C H C l3

HPLC !U V

BuB

E thyl ethe r

1610

ETHYL ETHER

0.01 - 0.2

0.25 - 3

C S2

G C -FID

CCT

E thyl ethe r

1610

ETHYL ETHER

0.01 - 0.2

0.25 - 3

Et Ac

G C !FID

CCT

Ethy l form ate

1452

ETHY L FO RM ATE

0.01 - 0.2

0.3 - 10

C S2

G C !FID

CCT

E thyl m e rc aptan

2542

M E R C A P TA N S

0.1 - 0.2

10 - 150

H C l/D C E

G C !FPD

GFF/HgAc

Ethy l me tha cryta te

2537

ME THYL a nd ETH YL M ETHA CR YLATE

0.01 - 0.05

1-8

C S2

G C -FID

XAD

F e nam ipho s

5600


0.2 - 1

12 - 240

t ol/a cet

G C !FPD

O VS !2

Fibrous glass

7400

A S BE ST O S & o th e r F IB ER S b y PC M

0.5 - 16

400 !va r ies

!

PCM

MC EF

Fluoranthene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Fluoranthene

5515


2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

Fluorene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Fluorene

5515


2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

F luo r ide s

7902

FLUORIDES, aerosol & ga s

1-2

12 - 800

N a OH

ISE

MCEF & pad w / N a2 C O 3

F luo r ide s

7906

FLU O RID ES by IC

1-2

s 1 - 800 i 120 - 800

N a OH

IC

MCEF & pad w/ N a 2C O 3

Fluorotrichloromethane

1006

F L UO R O T R IC H L O R O M E T H A NE

0.01 - 0.05

0.3 - 7

C S2

G C !FID

C CT ( lg )

F o no fo s

5600


0.2 - 1.0

12 - 240

t ol/a cet

G C !FPD

O VS !2

F o r malde hyde

2016

F O R M A L D E HY D E

0.1 - 1.5

1 - 15

ac eto nitr ile

HP LC - U V

SG/DNPH

F o r malde hyde

2541


0.01 - 0.1

1 - 36

t ol

G C !FID

X A D !2 /H M P

F o r malde hyde

3500


0.2 - 1.0

1 - 100

NaHSO 3

VIS

P TF E & 2 IM P

F o r malde hyde

2539


0.01 - 0.05

5-5

t ol

G C !F ID /M S

X A D !2 /H M P

F o r malde hyde

3800


0.1 - 2.0

Inst r. d ep .

NA

FTIR

Di r. R e a d

F o r malde hyde

5700

FORM ALDEHYDE on dust

2

240 - 1050

H 2O /D N PH /C H 3C N

HPLC !U V

I O M / P VC

F o rm e ta n ate .H C I

5601


0.1 - 1

var-480

reagent

HP LC , U V

OV S-2

Fo rm ic a cid

2011

FO RM IC A C ID

0.05 - 0.2

1 - 24

H 2O

IC

PTFE & SG ( w a sh e d )

F ur fur al

2529

FU R FU R AL

0.01 - 0.05

1 - 12

t ol

G C !FID

X A D !2 /H M P

F ur fur al

2539


0.05

5-5

t ol

G C !F ID /M S

X A D !2 /H M P

3/15/2003

MF!11


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max F u r fur yl alco ho l

2505

F UR FU RY L A LC O H O L

0.01 - 0.05

3 - 25

a cet

G C !FID

Por Q

G allium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

G lutar alde hyde

2532

G L U TA R A LD E H Y D E

0.01 - 0.08

4 - 39

C H 3C N

HPLC !U V

SG/DNPH

Glycerin mist

0500


1-2

7 - 133

NA

Grav

P VC

G lyc ido l

1608

G LY C ID O L

0.01 - 1.0

5 - 100

T HF

G C !FID

CCT

G lyc ols

5523

GLYC OLS

0.5 - 2

5 - 60

MeOH

G C !FID

O VS !7

G old

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

H eptanal

2539


0.01 - 0.05

5-5

t ol

G C !F ID /M S

X A D !2 /H M P

n !Heptane

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

n !Heptane

1500


0.01 - 0.2

NA

C S2

G C !FID

CCT

2-Heptanone

2553

KE TO NE S II

0.01 - 0.2

1 - 25

IP A -C S 2

G C -FID

A -C M S

3-Heptanone

2553

KE TO NE S II

0.01 - 0.2

1 - 25

IP A -C S 2

G C -FID

A -C M S

H er bic ides

5602


0.2 - 1

12 - 480

reagent

G C /E C D

OV S-2

H er bic ides

9200


NA

NA

NA

G C - EC D

polyethylene bag

H er bic ides

9201


NA

NA

IPA/diazomethane

G C - EC D

PUF pad

Hexachlorobutadiene

2543

H E X A C H LO R O B U T A D IE N E

0.05 - 0.2

1 - 100

hexane

G C !E C D

X A D !2

Hexa chloro !1,3 !cy clo pentadiene

2518

HEXACHLOR O !1,3 !CY CLO PEN TA D I EN E

0.01 - 0.2

0.25 - 90

hexane

G C !E C D

2 Por T

Hexachloroethane

1003


0.01 - 0.2

3 - 70

C S2

G C !FID

CCT

Hexamethylene! diisoc ya nate

5522

ISOCYANATES

1-2

15 - 360

tryptamine/DMSO

HPLC !FL

IM P

1,6-Hexamethylene ! diisoc ya nate

5521

ISO C YA NA TES , M O NO M ER IC

1.0

5 - 500

rea ge nts

HPLC !EC HD

IM P

1,6-Hexamethylene diiso cy an ate (HD I)

5525

ISOCYANATES, TOTAL (MAP)

1-2

1 - 500

MAP

HP LC /UV

G F F, IM P

H exanal

2539


0.01 - 0.05

5-5

t ol

G C !F ID /M S

X A D !2 /H M P

H exanal

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

n !Hexane

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

n !Hexane

1500


0.01 - 0.2

4-4

C S2

G C !FID

CCT

n-Hexane

3800


0.1 - 2.0

Inst r. d ep .

NA

FTIR

Di r. R e a d

2 !Hexanone

1300

KETONES I

0.01 - 1.0

1 - 10

C S2

G C !FID

CCT

2-Hexanone

2555

KETONES I

0.01 - 0.2

1 - 10

C S2

G C -FID

A -C M S

Hip pu ric ac id

8301

HIP PU RIC an d M ETH YL H IPP UR IC ACID in urine

NA

NA

Et a c

HP LC - U V

NA

Hydrazine

3503

H Y D R A ZI N E

0.2 - 1.0

7 - 100

rea ge nts

VIS

BuB

H y dr o ge n br o mide

7903


0.2 - 0.5

3 - 100

H C O 3 /C O 3

2-

H y dr o ge n c hlo r ide

7903


0.2 - 0.5

3 - 100

H C O 3-/C O 3

2-

H y dr o ge n c yanide

6010


0.05 - 0.2

2 - 90

H 2O

VIS

s od a lim e

H y dr o ge n c yanide

6017


0.05 - 2

2 - 90

H 2O

IC -D C Am p

SL

3/15/2003

MF!12

-

IC

SG

IC

SG


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max H ydr o ge n c yanide

7904

CYANIDES, AEROSOL & G AS

0.5 - 1.0

7 - 100

KOH

H y dr o ge n flo ur ide

7903


0.2 - 0.5

3 - 100

H C O 3 /C O 3

ISE

MC EF

IC

SG


7902

FLUORIDES, AEROSOL & G AS

1-2

12 - 800

N a OH

ISE

M CE F & p a d w / N a2C O 3


7906

FLU O RID ES by IC

1-2

1 - 800

N a OH

IC


H y dr o ge n sulfide

6013

H Y D R O G E N S UL F ID E (withdrawn)

0.1 - 1.5

1.2 - 40

N H 4OH /H 2O 2

IC

P T FE & C CT ( lg )

Hydroquinone

5004

H Y D R O Q U IN O N E

1-4

30 - 180

ac etic ac id

HPLC !U V

MC EF

Indeno[1,2,3-cd]pyrene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Inden o [1,2,3 !cd] pyrene

5515


2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

Iodine

6005

I O D IN E

0.5 - 1.0

15 - 225

N a 2C O 3

IC

C C T w /alk ali

I ndium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

I ron

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

I ron

7301


1-4

5 - 100

H C l /H N O 3

ICP-AES

MC EF

I ron

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

I ron

7300


1-4

5 - 100

H N O 3/HC lO 4

IC P !AES

MC EF

Isoa my l ace tate

1450

ESTERS I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

I soam yl alc o ho l

1402

ALC O HO LS III

0.01 - 0.2

1 - 10

IP A /C S 2

G C !FID

CCT

-

2-

I soam yl alc o ho l

1405

ALCOHO LS COM BINED

0.01 - 0.2

1 - 10

IP A -C S 2

G C -FID

CCT

Isob utyl a ce tate

1450

ESTERS I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

I sobutyl alco ho l

1401

ALC O HO LS II

0.01 - 0.2

2 - 10

IP A /C S 2

G C !FID

CCT

I sobutyl alco ho l

1405

ALCOHO LS COM BINED

0.01 - 0.2

2 - 10

IP A -C S 2

G C -FID

CCT

I sobutyraldehyde

2539


0.01 - 0.05

5-5

t ol

G C !F ID /M S

X A D !2 /H M P

I soc yanate s

5521


1.0

5 - 500

rea ge nts

HPLC !EC HD

IM P

I soc yanate s

5522

ISOCYANATES

1-2

15 - 360

tryptamine/DMSO

HPLC !FL/EC HD

IM P

Isophorone

2508

I SO P H O R O N E

0.01 - 1.0

2 - 25

C S2

G C !FID

PCT

Isophorone

2556

I SO P H O R O N E

0.01 - 1

2 - 25

DEE

G C -FID

XAD

Isop ho rone diisoc ya nate (IPD I)

5525


1-2

1 - 500

MAP

HP LC /UV

G F F, IM P

Isop rop yl ac etate

1454

ISOP RO PYL A CE TATE

0.02 - 0.2

0.1 - 9

C S2

G C !FID

CCT

Isop rop yl ac etate

1460


0.02 - 0.2

0.1 - 9

C S 2-M eth

G C -FID

CCT

I sopr o pyl alco ho l

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

I sopr o pyl alco ho l

1400

ALCOHO LS I

0.01 - 0.2

0.2 - 3

2 -b u ta n on e /C S 2

G C !FID

CCT

I sopr o pyl e the r

1618

ISOPROPYL ETHER

0.01 - 0.05

0.1 - 3

C S2

G C !FID

CCT

I sopr o pyl glyc idyl ether

1620

ISOPROPYL GLYCIDYL ETHER

0.01 - 0.2

1 - 30

C S2

G C !FID

CCT

I sovale r alde hyde

2018

ALIPHATIC ALDEHYDES

0.1 - 1.5

1 - 15

ACN

HP LC /UV

SG-DNPH

I sovale r alde hyde

2539


0.01 - 0.05

5-5

t ol

G C !F ID /M S

X A D !2 /H M P

Kepone

5508

KEPONE

0.5 - 1.0

50 - 600

b z/M e O H

G C !E C D

M C E F & IM P

Kerosene

1550

NAPHTHAS

0.01 - 0.2

1.3 - 20

C S2

G C !FID

CCT

3/15/2003

MF!13


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Lanthanum

7301


1-4

5 - 1000

H C l /H N O 3

ICP-AES

MC EF

La nthanum

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

Lead

7082

LEAD by FAAS

1-4

200 - 1500

H N O 3/H 2O 2

FAAS

MC EF

Lead

7702

LEAD BY FIELD POR TABLE XRF

1-4

570 - 1900

NA

XR F (po rt)

MC EF

Lead

7105

LEAD by GFAAS

1-4

1 - 1500

H N O 3/H 2O 2

G FAAS

MC EF

Lead

7701

LEAD BY ULTRASOUND /ASV

1-4

20 - 1500

HNO3

Port ASV

MC EF

Lead

7300


1-4

1250 -2000

H N O 3/HC lO 4

IC P !AES

MC EF

Lead

7700

LEAD in Air by Che mical Spot Test

2

10 - 240

!

Sp ot

MC EF

Lead

9100

LEAD in Surface Wipe Sa mp les

NA

NA

H N O 3/HC lO 4

A A S; IC P

Wipes

Lead

7301


1-4

50 - 2000

H C l /H N O 3

ICP-AES

MC EF

Lead

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

Lead

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Lead

9105

LEAD in DUST WIPES by C h emica l Spot Test

NA

NA

NA

Sp ot

Wipe

Lead sulfide

7505

L E AD S U LF ID E

1.7 or 2 .2

600 - 1000

T HF

XR D

C Y C & P VC

Limonene

1552

TERPENES

0.01 - 0.2

2 - 30

C S2

G C !FID

CCT

Limonene

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Lindane

5502

A L D R IN a n d LI N DA N E

0.2 - 1.0

18 - 240

isooctane

G C !E C N

GFF & BuB

Lithium

7300


1-4

100 - 2000

H N O 3/HC lO 4

IC P !AES

MC EF

Lithium

7301


1-4

100 - 2000

H C l /H N O 3

ICP-AES

MC EF

Lithium hydr o xide

7401

ALKA LINE DU STS

1-4

70 - 1000

HCl

T it ra t ion

PTFE

M agne sium

7300


1-4

5 - 67

H N O 3/HC lO 4

IC P !AES

MC EF

M agne sium

7301


1-4

5 - 67

H C l /H N O 3

ICP-AES

MC EF

M agne sium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

M alathio n

5600


0.2 - 1

12 - 60

t ol/a cet

G C !FPD

O VS !2

M ale ic A nhydride

3512

M A L E IC A N H Y D R ID E

0.2 - 1.5

40 - 500

H 2O

HPLC !U V

BuB

M ane b

3601

MANEB

NA

NA

NA

HP LC - U V

Hand wa sh

M ane b

3600

MANEB

NA

NA

Cy s/EDTA

HP LC - U V

Patch

Mang anese

7300


1-4

5 - 200

H N O 3/HC lO 4

IC P !AES

MC EF

Mang anese

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

Mang anese

7301


1-4

5 - 200

H C l /H N O 3

ICP-AES

MC EF

Mang anese

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

MBK

1300

KETONES I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

MDI (4,4'!methylene ! b isphe nyl iso c yanate )

5521


1.0

5 - 500

rea ge nts

HPLC !EC HD

IM P

MDI (4,4'!methylene ! b isphe nyl iso c yanate )

5522

ISOCYANATES

1-2

15 - 360

tryptamine

HPLC !FL/EC HD

IM P

Me rcury

6009

MER CURY

0.15 - 0.25

2 - 100

H N O 3/H C l

AAS !cold va p

Ho pc alite

3/15/2003

MF!14


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Mercaptans

2542

M E R C A P TA N S

0.1 - 0.2

10 - 150

H C l/D C E

G C !FPD

GFF/HgAc

M e sityl o xide

1301

KE TO NE S II

0.01 - 0.2

1 - 25

M e O H /C S 2

G C !FID

CCT

M e sityl o xide

2553

KE TO NE S II

0.01 - 0.2

1 - 25

IP A -C S 2

G C -FID

A -C M S

M eta ls in air

7300


1-4

var - 2000

H N O 3/HC lO 4

IC P !AES

MC EF

M e talwo r k ing F luids

5524

META LWO RKING FLUIDS (MW F) ALL CATEGO RIES

1.6 - 2.0

1000 - ND

D C M/MeO H/T ol MeOH

Grav

PTFE/CYC

M e thanal

2016


0.1 - 1.5

1 - 15

ac eto nitr ile

HP LC - U V

SG/DNPH

M e tham ido pho s

5600


0.2 - 1

12 - 240

t ol/a cet

G C !FPD

O VS !2

M e thano l

2000

M E TH A NO L

0.02 - 0.2

1-5

H 2O/IPA

G C -FID

SG

M e thano l

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

M e thano l

3800


0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

Me thioca rb

5601


0.1 - 1

var - 480

reagent

HP LC - U V

OV S-2

Methomyl

5601


0.1 - 1

var - 480

reagent

HP LC - U V

OV S-2

M e to lac hlo r

5602


0.2 - 1

12 - 480

reagent

G C /E C D

OV S-2

M e to lac hlo r

9200


NA

NA

NA

G C - EC D

polyethylene bag

M e to lac hlo r

9201


NA

NA

IPA/diazomethane

G C - EC D

PUF pad

2 !M etho xye thyl a ce tate

1451

ME THYL C ELLO SO LVE A CE TATE

0.01 - 0.2

0.2 - 20

C S2

G C !FID

CCT

2 !M e tho xye thano l

1403

ALC O HO LS IV

0.01 - 0.05

6 - 50

M e O H /C H 2C l2

G C !FID

CCT

M ethy l ace tate

1458

ME THYL A CE TATE

0.01 - 0.2

0.2 - 10

C S2

G C !FID

CCT

M ethy l acry late

1459

ME THYL A CR YLATE

0.01 - 0.2

1-5

C S2

G C !FID

CCT

M ethy l acry late

2552

ME THYL A CR YLATE

0.01 - 0.2

1-5

C S2

G C -FID

A -C M S

M e thyl alco ho l

2000

M E TH A NO L

0.02 - 0.2

1-5

H 2O/IPA

G C !FID

SG

M e thylal

1611

METHYLAL

0.01 - 0.2

1-3

hexane

G C !FID

CCT

4-M eth ylb en ze ne su lfon ic ac id

5043

p -TO LUE NE SU LFO NIC AC ID

1-3

10 - 1000

IPA/H 20

HP LC - U V

GFF

N -Methyl-y-butyrolactone

1302

N - M E TH Y L -2 - PY R R O L ID I NO N E

0.05 - 0.2

0.5 - 125

C H 2C l2/M e O H

G C -NP D o r FID

CCT

Methyl !(n !am yl) !ketone

1301

KE TO NE S II

0.01 - 0.2

1 - 25

M e O H /C S 2

G C !FID

CCT

M eth yla rso nic ac id

5022


1-3

50 - 1000

b u ffer

IC !HYAAS

PTFE

M e thyl br o m ide

2520

M E T H YL B RO M I D E

0.01 - 0.1

1-5

C S2

G C !AED

P C T (2 ) +d ry t u b e CCT CCT

Methyl cellosolve

1403

ALC O HO LS IV

0.01 - 0.05

6 - 50

M e O H /C H 2C l2

G C !FID

M ethy l celloso lve a ce tate

1451


0.01 - 0.2

0.2 - 20

C S2

G C !FID

M e thyl c hlo r ide

1001

M E T H YL C H LO R I D E

0.01 - 0.1

0.4 - 3

C H 2C l2

G C !FID

2 C C T (lg + sm )

Me thyl chloro form

1003


0.01 - 0.2

0.1 - 8

C S2

G C !FID

CCT

Me thyl chloro form

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

M e thyl c yanide

1606

AC ETON ITRILE

0.01 - 0.2

3 - 25

MEC l/MEO H

G C !FID

CCT

Methyl cyclohexane

1500


0.01 - 0.2

4-4

C S2

G C !FID

CCT

M e thylc yc lo he xano l

1404

M E TH YL CY C LO H EX AN O L

0.01 - 0.2

1 - 15

C H 2C l2

G C !FID

CCT

Methylcyclohexanone

2521

M E T H YL C Y C LO H E X A N O N E

0.01 - 0.05

1-6

a cet

G C !FID

Por Q

4,4 '-M eth yle ne -b is (c yc lo he xyl iso cy an ate ) (HM DI)

5525


1-2

1 - 500

MAP

HP LC /UV

G F F, IM P

3/15/2003

MF!15


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max 4,4-Methylene-bis (phenyl isoc ya na te) (M DI)

5525


1-2

1 - 500

MAP

HP LC /UV

G F F, IM P

M e thyle ne c hlo r ide

1005


0.01 - 0.2

0.5 - 2.5

C S2

G C -FID

2 CCT


2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD


3800


0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

4,4'!Methylenedianiline

5029

4,4'!M E T H YL E N ED I AN I LI N E

1-2

10 - 1000

K O H/M e O H

HPLC !U V

GF F/H 2SO 4

4,4 !Methylene diphenyl diisoc ya nate

5522

ISOCYANATES

1-2

15 - 360

tryptamine

HPLC !FL/EC HD

IM P

Methyl ethyl ketone

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Methyl ethyl ketone

2500


0.01 - 0.2

0.25 - 12

C S2

G C !FID

Carbon be ads

Methyl ethyl ketone

2555

KETONES I

0.01 - 0.2

1 - 10

C S2

G C -FID

A -C M S

Methyl ethyl ketone p er o xide

3508

M E T H YL E TH Y L K E TO N E P E R O X ID E

0.5 - 0.2

52 - 520

reagent

VIS

IM P

5 !Methyl !3 !heptanone

1301

KE TO NE S II

0.01 - 0.2

1 - 25

M e O H /C S 2

G C !FID

CCT

5-Methyl-3-heptanone

2553

KE TO NE S II

0.01 - 0.2

1 - 25

IP A -C S 2

G C -FID

A -C M S

M eth yl h ipp ur ic a cid

8301

HIP PU RIC an d M ETH YL H IPP UR IC ACID in urine

NA

NA

Et a c

HP LC - U V

NA

M e thyl io dide

1014

M E T H YL IO D I D E

0.01 - 1.0

15 - 50

t ol

G C !FID

CCT

M ethy l isoam yl ac etate

1450

ESTERS I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

M e thyl iso butyl c ar binol

1402

ALC O HO LS III

0.01 - 0.2

1 - 10

IP A /C S 2

G C !FID

CCT

M e thyl iso butyl c ar binol

1405

ALCOHO LS COM BINED

0.01 - 0.2

1 - 10

IP A -C S 2

G C -FID

CCT

Methyl isobutyl ketone

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD


1300

KETONES I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT


2555

KETONES I

0.01 - 0.2

1 - 10

C S2

G C -FID

A -C M S

M e thyl me r c aptan

2542

M E R C A P TA N S

0.1 - 0.2

10 - 150

H C l/D C E

G C !FPD

GFF/HgAc

M ethy l me tha cryla te

2537


0.01 - 0.05

1-8

C S2

G C !FID

XAD

M e thyl par athio n

5600


0.2 - 1

12 - 240

t ol/a cet

G C !FPD

O VS !2

M e thyl phe no l

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

N -methyl-2-pyrrolidinone

1302


0.05 - 0.2

0.5 - 125

C H 2C l2/M e O H

G C -NP D o r FID

CCT

"!Methyl styrene

1501


0.01 - 0.2

1 - 30

C S2

G C !FID

CCT

$ -Methylstyrene

1501


0.01 - 0.2

1 - 30

C S2

G C -FID

CCT

M eth yl tert !butyl e ther

1615

METH YL tert !BUTYL ETHER

0.1 - 0.2

2 - 96

C S2

G C !FID

2 CC T ( lg )

M e thyltin c hlo r ide

5526

METHYLTIN CHLORIDES

0.25 - 1

15 - 75

AAA

GC-FPD

O VS

M e vinphos

5600


0.2 - 1.0

12 - 240

t ol/a cet

G C !FPD

O VS !2

M inera l spirits

1550

NAPHTHAS

0.01 - 0.2

1.3 - 20

C S2

G C !FID

CCT

M o lybde num

7300


1-4

5 - 67

H N O 3/HC lO 4

IC P !AES

MC EF

M o lybde num

7301

EL EM EN TS b y IC P (A qu a R eg ia Ashin g)

1-4

5 - 67

H C l /H N O 3

ICP-AES

MC EF

M o lybde num

7303

EL EM EN TS b y IC P (H ot B loc k/H C l/ H N O 3 Digestion)

1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

M o lybde num

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

M o no c r o to pho s

5600


0.2 - 1

12 - 240

t ol/a cet

G C !FPD

O VS !2

3/15/2003

MF!16


Chemical

M eth No.


M e th od Na m e

Vol. (L)

E x tr a c ti o n


Sampler

min max Monom ethylaniline

3511

M O N O M E T HY L AN I LI N E

0.2 - 1.0

11 - 100

N a OH

G C !FID

BuB /H 2SO 4

Monom ethylhydrazine

3510

M O N O M E T HY L H YD R A Z IN E

0.5 - 1.5

3 - 20

P M A /H C l

VIS

B u B/H C l

M yc o bac te rium

0900

M YC O BA C TER IUM TUB ER C ULO SIS

$4

va r ies

PCR

reagent

PTFE

Nap htha (coal tar)

1550

NAPHTHAS

0.01 - 0.2

1.3 - 20

C S2

G C !FID

CCT

Naphthalene

1501


0.01 - 1.0

100 - 200

C S2

G C !FID

CCT

Naphthalene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Naphthalene

5515


2.0

200 - 1000

va r ies

1,5-Naphthalene diiso cy an ate (ND I)

5525


1-2

1 - 500

MAP

HP LC - U V

G F F, IM P

N a phthylamine s

5518

NAPHTHYLAMINES

0.2 - 0.8

30 - 100

acetic a /IPA

G C !FID

GFF & SG

N eo dym ium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

N i c ke l

7300


1 !4

25 - 1000

H N O 3/HC lO 4

IC P !AES

MC EF

N i c ke l

7301


1-4

5 - 1000

H C l /H N O 3

ICP-AES

MC EF

N i c ke l

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

N i c ke l

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

G C -FID

P T F E & X A D !2

Nickel carbonyl

6007

NICKEL CARBONYL

0.05 - 0.2

7 - 80

HNO3

G FAAS

C C T (lo w N i)

Nicotine

2544

N I C O TI N E

1.0

60 - 400

Et Ac

G C !NPD

X A D !2

Nicotine

2551

N I C O TI N E

0.1 - 1.0

0.5 - 600

ethy l ace tate

Nit ric ac id

7903


0.2 - 0.5

3 - 100

H C O 3-/C O 3

N i tr ic o xide

6014

N I TR IC O X I D E & N IT R O G E N D IO X I D E

0.025

1.5 - 6

p !Nitroaniline

5033

p !N I TR O A N IL IN E

1-3

20

Nitrobenzene

2005


0.01 - 1

10 - 150

MeOH

G C !FID

SG

Nitrobenzene

2017


0.2

5 - 50

et h a nol

G C -FID

GFF + SG

N i tr o be nzo l

2017


0.2

5 - 50

et h a nol

G C -FID

GFF + SG

p !Nitrochlorobenzene

2005


0.01 - 1

1 - 150

MeOH

G C !FID

SG

Nitroethane

2526

N I TR O E T H AN E

0.01 - 0.05

1.5 - 3

Et Ac

G C !FID

2 X A D !2

N i tr o ge n dio xide

6014


0.025 - 0.2

1.5 - 6

reagent

VIS

MS w/TEA

N i tr o ge n dio xide

6700

N I TR O G E N D IO X I D E

NA

NA

reagent

VIS

Diffusive

N i tr o ge n pe r o xide

6700

N I TR O G E N D IO X I D E

NA

NA

reagent

VIS

Diffusive

Nit ro gly ce rin

2507


0.2 - 1.0

3 - 100

et h a nol

G C !E C D

T e n a x!G C

Nitromethane

2527

N I TR O M E T H A N E

0.01 - 0.05

1.2 - 3

Et Ac

G C !FPD

Chrom 106

2 !Nitropropane

2528

2 !N I TR O P R O P A N E

0.01 - 0.05

0.1 - 2

Et Ac

G C !FID

Chrom 106

1-Nitropyrene

2560

1-NITROPYRENE in DIESEL PARTICULATES

1.0 - 2.0

480 - 960

T ol

G C /N C D

GFF

N i tr o samine s

2522

NITROSAMINES

0.2 - 2.0

15 - 1000

M e O H /C H 2C l2

G C !TEA

T D tu b e

o - ,m - , p -Nitrotoluene

2005


0.01 - 0.2

1 - 30

MeOH

G C !FID

SG

N i tr o us o xide

3800


0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

3/15/2003

MF!17

GC-NPD

XA D-4

IC

S G ( w a s h ed )

reagent

VIS

M S w / T EA & o x id i ze r

IPA

HPLC !U V

MC EF

2-


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Nitr o us o xide

6600

N I TR O U S O X ID E

NA

80% vol

NA

IR

air bag

n-Nonane

1500

HYDROC ARBONS, BP 36-216 oC

0.01 - 0.2

4-4

C S2

G C -FID

CCT

NMP

1302

N-Methyl-2-Pyrrolidinone

0.05 - 0.2

0.5 - 125

C H 2C l2/M e O H

GC-FID/NPD

CCT

Nuisance dusts

0500


1-2

7 - 133

NA

G R AV

P VC

n !Octane

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

n !Octane

1500


0.01 - 0.2

4-4

C S2

G C !FID

CCT

Oc tam ethylcy clotetra ! siloxane

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

1 !Oc tane thio l

2510

1 !O C TA N ETH IO L

0.01 - 0.2

1 - 15

a cet

G C !FPD

Te na x G C

O il m ist (m ine ra l)

5026

OIL MIST, MINER AL

1-3

20 - 500

C C l4

IR

PVC or MCE

O r gano nitro ge n pe sticides

5601


0.1 - 1

varies-480

reagent

HP LC - U V

OV S-2

O r gano pho spho r us Pestic ide s

5600


0.2 - 1

12 - 240

t ol/a cet

G C !FPD

O VS !2

Oxamyl

5601


0.1 - 1

var - 480

reagent

HP LC , U V

OV S-2

O xyge n

6601

OXYG EN

NA

1 - NA

NA

Sens or

po rta ble

PA C

5800

POLY AROM ATIC COMPO UNDS, TOTAL (PACs)

1-2

5 - 1000

hexane

FI-FL

PTFE + X AD -2

Palladium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Par aquat

5003

PARAQUAT

1-4

40 - 1000

H 2O

HPLC !U V

PTFE

Par athio n

5600


0.2 - 1.0

12 - 240

t ol/a cet

G C !FPD

O VS !2

Par tic ulate s N . O. R.

0500

PARTICU LATES N.O.R ., TO T AL

1-2

7 - 133

NA

G R AV

P VC

Par tic ulate s N . O. R.

0600

PARTICU LATES, N.O .R, RESPIRAB LE

1.7, 2.2, 2.5

20 - 400

NA

Grav.

C Y C & P VC

Pentachlorobenzene

5517

POLYCHLORO BENZENES

0.01 - 0.2

3 - 12

hexane

G C !E C D

P T F E & X A D !2

Pentachloroethane

2517

P E N TA C H L O R O E TH A N E

0.01 - 0.2

1 - 10

hexane

G C !E C D

Por R

Pe ntac hlo r o phe no l

5512

P EN TA C HL OR O PH EN O L

0.5 - 1.0

48 - 480

MeOH

HPLC !U V

MCEF & BuB

Pentamidine

5032

PEN TAM IDINE ISETH ION ATE

1-2

50 - 1500

rea ge nts

HPLC/FL

P VC / o p a q u e

n !Pentane

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

n !Pentane

1500


0.01 - 0.2

4-4

C S2

G C !FID

CCT

2 !Pentanone

1300

KETONES I

0.01 - 2.0

1 - 10

C S2

G C !FID

CCT

2-Pentanone

2555

KETONES I

0.01 - 0.2

1 - 10

C S2

G C -FID

A -C M S

Perchloroethylene

3704

PE RC HL O RO ETH YL EN E (p or t G C ) in exha led bre ath a nd a ir

0.02 - 5

< 80% ca p

NA

G C (po rt)-PID

air bag

Perchloroethylene

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Pe stic ide s

5600


0.2 - 1

12 - 240

t ol/a cet

G C !FPD

O VS !2

Pe stic ide s

5601


0.1 - 1

var - 480

reagent

HP LC - U V

OV S-2

Pe tro leum e the r/naphtha

1550

NAPHTHAS

0.01 - 0.2

1.3 - 20

C S2

G C !FID

CCT

Phenanthrene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Phenanthrene

5515


2.0

200 - 1000

va r ies

G C -FID

P T F E & X A D !2

Phe no l

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

3/15/2003

MF!18


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Phe no l

2546

C R ES O LS an d P HE NO L

0.01 - 0.1

1 - 24

MeOH

G C !FID

X A D !7

Phe nyl e the r

1617

PHENYL ETHER

0.01 - 0.2

1 - 50

C S2

G C !FID

CCT

Phe nyl e the r!diphenyl mixture

2013

PHENYL ETHER !DIPHENYL MIXT U R E

0.01 - 0.2

1 - 40

bz

G C !FID

SG

Phe nyl glyc idyl ethe r

1619

PHENYL GLYCIDYL ETHER

0.01 - 1

80 - 150

C S2

G C !FID

CCT

Phenylhydrazine

3518

P H E N YL H Y DR A Z IN E

0.2 - 1.0

25 - 120

PMA

VIS

B u B/H C l

Pho rate

5600


0.2 - 1

12 - 240

t ol/a cet

G C !FPD

O VS !2

Phosdrin (mevinphos)

5600


0.2 - 1

12 - 480

t ol/a cet

G C !FPD

O VS !2

Phosphine

6002

P H O S P H IN E

0.01 - 0.2

1 - 16

reagent

VIS

S G / H g( C N )2

-

2-

Ph os ph or ic a cid

7903


0.2 - 0.5

3 - 100

H C O 3 /C O 3

IC

S G ( w a s h ed )

Pho spho rus

7300


1-4

50 - 2000

H N O 3/HC lO 4

IC P !AES

MC EF

Pho spho rus

7905

PHOSPHOR U S

0.01 - 0.2

5 - 100

xylene

G C !FPD

Te na x G C

Pho spho rus

7301


1-4

25 - 2000

H C l /H N O 3

ICP-AES

MC EF

Pho spho rus

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Pho spho rus

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

Pho spho rus tr ic hlor ide

6402

P H O S P H O R U S T R IC H L O R ID E

0.05 - 0.2

11 - 100

rea ge nts

VIS

BuB /H 2O

Pinene

1552

TERPENES

0.01 - 0.2

2 - 30

C S2

G C !FID

CCT

Pinene

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Pla tinum

7300


1-4

13 - 2000

H N O 3/HC lO 4

IC P !AES

MC EF

PA H

5506


2.0

200 - 1000

va r ies

HPLC !FL/U V

P T F E & X A D !2

Poly ac rylate

5035

SUPER ABSORBENT POLYMER

1-2

50 - 1500

C u (Ac)2

IC P or AAS

P VC

PACs

5800

PO LYC YC LIC AR O M ATIC COM POU NDS, TOTAL

1-2

5 - 1000

hexane

FI-FL

Platinum

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Po lyc hlo ro bip he ny l (42 % & 5 4% C l)

5503


0.05 - 0.2

1 - 50

hexane

G C !E C D

G FF & F lor isil

Po tassium

7301


1-4

5 - 1000

H C l /H N O 3

ICP-AES

MC EF

Po tassium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Po tassium hydr o xide

7401

ALKA LINE DU STS

1-4

70 - 1000

HCl

t it ra t ion

PTFE

Progesterone

5044


1

150 - 1000

M eth

HP LC - U V

PTFE

Propazine

8315


NA

NA

NA

GC-M SD

Urine

Pr o pham

5601


0.1 - 1

var - 480

reagent

HP LC , U V

OV S-2

Pr o pio nalde hyde

2539


0.01 - 0.05

5-5

t ol

G C !F ID /M S

X A D !2 /H M P

Pr o pio nalde hyde

2018

ALIPHATIC ALDEHYDES

0.1 - 1.5

1 - 15

ACN

HP LC - U V

SG-DNPH

Pr o po xur

5601


0.1 - 1

var - 480

reagent

HP LC , U V

OV S-2

n !Prop yl ac etate

1450

ESTERS I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

n !Pr o pyl alc o ho l

1401

ALC O HO LS II

0.01 - 0.2

1 - 10

IP A /C S 2

G C !FID

CCT

n- Pro pyl alco ho l

1405

ALCOHO LS COM BINED

0.01 - 0.2

1 - 10

IP A -C S 2

G C -FID

CCT

Pr o pyle ne dic hlor ide

1013


0.01 - 0.2

0.1 - 3.5

a cet /cy ch ex

G C !E C N

PCT

3/15/2003

MF!19


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Pro pyle ne glyc o l

5523

GLYC OLS

0.5 - 2

5 - 60

MeOH

G C !FID

O VS !7

Pr o pyle ne glyc o l m o no m e thyl e the r

2554

GLYCOL ETHER S

0.1 - 0.2

3 - 25

M e C l2/Me th

G C -FID

A-747

Pr o pyle ne glyc o l mo nom ethy l ethe r ac etate

2554

GLYCOL ETHERS

0.1 - 0.2

3 - 25

M e C l2/Me th

G C -FID

A-747

Pr o pyle ne o xide

1612


0.01 - 0.2

0.5 - 5

C S2

G C !FID

CCT

Pyrene

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

Pyrene

5515


2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

Pyr e thr um

5008

PYRETHUM

1-4

20 - 400

C H 3C N

HPLC !U V

GFF

Pyridine

1613

P Y R ID I NE

0.01 - 1.0

18 - 150

C H 2C l2

G C !FID

CCT

R eso rc ino l

5701

R ES O RC IN O L

0.2 - 1

5 - 160

MeOH

G C -FID

OV S-7

Rib av irin

5027

RIB AV IRIN

1-4

5 - 1000

H 2SO 4

HPLC !U V

GFF

R onne l

5600


0.2 - 1

12 - 60

t ol/a cet

G C !FPD

O VS !2

Rotenone

5007

ROTENONE

1-4

8 - 400

C H 3C N

HPLC !U V

PTFE

Rubber solvent

1550

NAPHTHAS

0.01 - 0.2

1.3 - 20

C S2

G C !FID

CCT

S e le nium

7300


1-4

5 - 2000

H N O 3/HC lO 4

IC P !AES

MC EF

S e le nium

7301


1-4

13 - 2000

H C l /H N O 3

ICP-AES

MC EF

S e le nium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

S e le nium

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

S ilic a, amo rpho us

7501

SILICA, AMOR PHOUS

1.7 or 2 .2

50 - 400

ash

XR D

PVC (total) PVC&C YC

Silica, crystalline

7500

SILICA, CRYSTALLINE, by XR D

1.7, 2.2, 2.5

400 - 1000

a s h or T HF

XR D

C Y C & P VC

Silica, crystalline

7601

S IL IC A , C R Y ST A LL IN E

1.7, 2.2, 2.5

400 - 800

H 3PO 4/HF

VIS

CYC & MC E or P VC

Silica, crystalline

7602

SILICA, CRYSTALLINE (IR )

1.7, 2.2, 2.5

400 - 800

ash

IR

CY C & M C E o r P VC

S ilic o n dio xide

7500

S IL IC A , C R Y ST A LL IN E , b y X R D.

1.7, 2.2, 2.5

400 - 1000

a s h or T HF

XR D

C Y C & P VC

Silica in coal mine dust

7603

QUA RTZ in coal mine dust

1.7, 2.2, 2.5

300 - 1000

ash

IR

C Y C & P VC

S ilve r

7300


1-4

250 - 2000

H N O 3+

IC P !AES

MC EF

S ilve r

7301


1-4

250 - 2000

H C l /H N O 3

ICP-AES

MC EF

S ilve r

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

Simazine

5602


0.2 - 1

12 - 480

reagent

G C /E C D

OV S-2

Simazine

9200


NA

NA

NA

G C - EC D

polyethylene bag

Simazine

9201


NA

NA

IPA/diazomethane

G C - EC D

PUF pad

S o dium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

S o dium hexa fluoro !alum inate

7902


1-2

12 - 800

N a OH

ISE

MCEF& pad w / N a2C O 3

3/15/2003

MF!20


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max S odium hexa fluoro !alum inate

7906

FLU O RID ES by IC

1-2

120 - 800

N a OH

IC


S o dium hydr o xide

7401

ALKA LINE DU STS

1-4

70 - 1000

HCl

T it ra t ion

PTFE

Stibine

6008

S T IB IN E

0.01 - 0.2

4 - 50

HCl

VIS

S G w /H g C l2

Stoddard solvent

1550

NAPHTHAS

0.01 - 0.2

1.3 - 20

C S2

G C !FID

CCT

S t ro ntium

7301


1-4

10 - 1000

H C l /H N O 3

ICP-AES

MC EF

S t ro ntium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

S t ro ntium

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

Strychnine

5016

S T RY C H N IN E

1-3

70 - 1000

rea ge nts

HPLC !U V

GFF

Styrene

1501


0.01 - 1.0

1 - 14

C S2

G C !FID

CCT

Styrene

3800


0.1 - 20

Inst r. D ep .

NA

FTIR

Di r. R e a d

S ulfur dioxide

6004

S U LF U R D IO X I D E

0.5 - 1.5

4 - 200

H C O 3-/C O 32-

IC


S ulfur he xafluo ride

6602

S U LF U R H EX A F LU O R ID E

0.01 - 0.05

80% vol

NA

Su lfur ic a cid

7903


0.2 - 0.5

3 - 100

H C O 3 /C O 3

S ulfuryl fluo r ide

6012

S U LF U R Y L F L UO R I D E

0.05 - 0.1

1.3 - 10

S ulpr o fo s

5600


0.2 - 1

12 - 240

S upe r abso rbe nt po lymer

5035


1-3

Simazine

8315


NA

2,4,5 !T

5001

2,4 !D an d 2,4,5 !T

TB

0900

T ellurium

G C !E C D

air bag

IC

SG(washed)

N a OH

IC

CC T ( lg )

t ol/a cet

G C !FPD

O VS !2

50 - 1500

C u (Ac)2

IC P or AAS

P VC

NA

NA

GC-M SD

Urine

1-3

15 - 200

MeOH

HPLC !U V

GFF

MYCO BACTERIUM TUBERCULOSIS, A IR B O R N E

$4

va r ies

reagent

PCR

PTFE

7300


1-4

25 - 2000

HNO3

IC P !AES

MC EF

T ellurium

7301


1-4

25 - 2000

H C l /H N O 3

ICP-AES

MC EF

T ellurium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

T ellurium

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

T erbufo s

5600


0.2 - 1

12 - 240

t ol/a cet

G C !FID

O VS !2

T erpe ne s

1552

TERPENES

0.01 - 2

2 - 30

C S2

G C !FID

CCT

o !Terphenyl

5021

o !TERPHENYL

1-3

2 - 30

C S2

G C !FID

PTFE

1,1,2,2 !Te tra bro m o ethane

2003


0.2 - 1.0

50 - 100

T HF

G C !FID

SG

Te tra bu tylt in

5504


1 - 1.5

50 - 500

aaa

HP LC /G FAAS

G F F & X A D !2

1,2,4,5 !Tetrachlorobenzene

5517

POLYCHLORO BENZENES

0.01 - 0.2

3 - 12

hexane

G C !E C D

P T F E & X A D !2

1,1,2,2 !Tetrach loro ! 2,2-difluoroethane

1016

1,1,2,2 !TETRACHLORO !2,2 ! DIFLUOROETHANE & 1,1,2,2 !TETR ACHLOR O !1,2 ! D I FL U O R O E TH A N E

0.01 -0.035

0.5 - 2

C S2

G C !FID

CCT

1,1,1,2 !Tetrach loro !1,2 -d iflu oroethane

1016


0.01 -0.035

0.5 - 2

C S2

G C !FID

CCT

1,1,2,2 !Tetrachloroethane

1019


0.01 - 0.2

3 - 30

C S2

G C !FID

PCT

1,1,2,2-Tetrachloroethane

2562

1 , 1, 2 ,2 - TE T RA C H L O R O E TH A N E

0.01 - 0.2

3 - 30

C S2

G C -FID

A -C M S

3/15/2003

MF!21

-

2-


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Tetrachloroethylene

1003


0.01 - 0.2

1 - 40

C S2

G C -FID

CCT

Tetrachloroethylene

3704

PE RC HL O RO ETH YL EN E (p or t G C ) in exha led bre ath a nd a ir

0.1 - 1

< 80% ca p

NA

Po rt G C -PID

air bag

T etr ae thyle ne glyc o l

5523

GLYC OLS

0.5 - 2

5 - 60

MeOH

G C !FID

O VS !7

T etr ae thyl lead

2533

TETR AETHYL LEAD (as Pb )

0.01 - 1.0

30 - 200

pentane

G C !PID

X A D !2

Tetra ethy l pyro ph osp ha te

2504

TETRA ETHY L PYRO PHO SPH ATE

0.01 - 0.2

20 - 48

toluene

G C !FPD

2 Chrom 102

Tetrafluoroethylene

3800


0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

T etr ahydro furan

1609

TETR AHYDR OFU R AN

0.01 - 0.2

1-9

C S2

G C !FID

CCT

T etr ahydro furan

3800


0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

Te tra kis (hy dr ox ym eth yl) p ho spho nium c hlo ride

5046

TETRKIS(HYDR OX YM ETHYL) P H O S P H O N IU M C H L O R ID E

1 - 1.7

1 - 400

ACN

HP LC - U V

GFF

T etr am e thyl lead

2534

TETRAMETHYL LEAD (as P b )

0.01 - 0.2

15 - 100

pentane

G C !PID

X A D !2

T etr am e thyl thio ur e a

3505

TETRAMETHYL THIOUREA

0.2 - 1.0

50 - 250

rea ge nts

VIS

IMP /H 2O

Tetranitromethane

3513

T E TR A N IT R O M E TH A N E

0.5 - 1.0

20 - 250

!

G C !FID

I M P /E t A c

T hallium

7300


1-4

25 - 2000

H N O 3/HC lO 4

IC P !AES

MC EF

T hallium

7310


1-4

25 - 2000

H C l /H N O 3

ICP-AES

MC EF

T hallium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Thiobe nca rb

5601


0.1 - 1

var - 480

reagent

HP LC , U V

OV S-2

Thiophenate-methyl

9205

CAPTAN and THIOPHENATE-METHYL o n D E RM A L P A TC H

NA

NA

IP A /A C N

HP LC - U V

Patch

Thiophenate-methyl

9202

CAPTAN and THIOPHENATE-METHYL in Hand Rinse

NA

NA

NA

HP LC - U V

Hand wa sh

Thiophenate-methyl

5606

THIO PH EN ATE -M ETH YL in AIR

0.1 - 1.0

20 - 480

IP A /A C N

HP LC - U V

QFF/SST

T hir am

5005

THIRAM

1-4

10 - 400

C H 3C N

HPLC !U V

PTFE

Tin

7301


1-4

5 - 1000

H C l /H N O 3

ICP-AES

MC EF

Tin

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Tin, organic compds as Sn

5504

ORG ANOTIN CPDS. (as Sn)

1 - 1.5

50 - 500

a c etic a /C H 3C N

HP LC /G FAAS

G F F & X A D !2

T itanium

7300


1-4

5 - 100

H N O 3/HC lO 4

IC P !AES

MC EF

T itanium

7301


1-4

5 - 100

H C l /H N O 3

ICP-AES

MC EF

T itanium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Toluene

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

Toluene

4000

TOLU ENE (Diffusive sam pler)

NA

15 min-8h

C S2

G C !FID

Diffusive

Toluene

1500


0.01 - 0.2

2-8

C S2

G C !FID

CCT

Toluene

1501


0.01 - 0.2

1-8

C S2

G C !FID

CCT

Toluene

3800


0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

2,4 & 2,6 !Toluenediamine

5516

2,4 ! & 2,6 !T O L UE N E D IA M I N E

1.0

30 - 500

a ce ty la te /M e O H

HPLC !U V

IM P

Toluene !2,4 !diisoc ya nate

2535

T O L UE N E !2,4 !DIISO CY ANA TE

0.2 - 1.0

2 - 170

MeOH

HPLC !U V

GW coated


5521


1.0

5 - 500


HPLC !EC HD

IM P

3/15/2003

MF!22


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Toluene !2,4 !diisoc ya nate

5522

ISOCYANATES

1-2

15 - 360

tryptamine/DMSO

HPLC !FL/EC HD

IM P

Tolue ne 2 ,4-d issoc ya nate (2,4 -TD I)

5525


1-2

1 - 500

MAP

HP LC - U V

G F F, IM P


5522

ISOCYANATES

1-2

15 - 360

tryptamine/DMSO

HPLC !FL/EC HD

IM P


5521


1.0

5 - 500


HPLC !EC HD

IM P

Tolue ne-2 ,6-d iisocy ana te (2,6 -TD I)

5525


1-2

1 - 500

MAP

HP LC - U V

G F F, IM P

p -To lue ne su lfon ic a cid

5043

P-TO LUE NE SU LFO NIC AC ID

1-3

10 - 1000

IPA/H 2O

HP LC - U V

GFF

o !Toluidine

2002


0.02 - 1.0

10 - 150

Et h a nol

G C !FID

SG

o !Toluidine

2017


0.2

5 - 50

et h a nol

G C -FID

GFF + SG

o !Toluidine

5013

DYES

1-3

150 - 500

H 2O

HPLC !U V

PTFE

o !Toluidine

8317

ANALINE an d o-TOLUIDINE in urine

NA

NA

ALK

H P LC - EC D

NA

o-Toluidine

8313

ANALINE an d o-TOLUIDINE in urine

NA

NA

ALK

H P LC - EC D

NA

Tribromomethane

1003


0.01 - 0.2

4 - 70

C S2

G C !FID

CCT

Tributy l pho sph ate

5034

TRIBUTY L PHO SPH ATE

1-3

2 - 100

d ieth y l et h er

G C !FPD

MC EF

T ri butyltin c hlo r ide

5504


1 - 1.5

50 - 500


HP LC /G FAAS

G F F & X A D !2

1,2,4 !Trichlorobenzene

5517

POLYCHLORO BENZENES

0.01 - 0.2

3 - 12

hexane

G C !E C D

P T F E & X A D !2

1,1,2 !Trichloroethane

1003


0.01 - 0.2

2 - 60

C S2

G C -FID

CCT


1003


0.01 - 0.2

0.1 - 8

C S2

G C -FID

CCT


2549


0.01 - 0.05

1-6

t h erma l

TD /G C -M S

TD

Trichloroethylene

1003


0.01 - 0.2

0.2 - 30

C S2

G C -FID

CCT

Trichloroethylene

1022

T R IC H L O R O E TH Y L EN E

0.01 - 0.2

1 - 30

C S2

G C -FID

CCT

Trichloroethylene

3701

TR IC H LO R O ETH YL EN E b y p ort G C

> 0.02

80% vol

NA

GC -port

air bag

Trichloroethylene

3800


0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

Trichlorofluoromethane

1006


0.01 - 0.05

0.3 - 7

C S2

G C -FID

CC T ( lg )

Trichloromethane

1003


0.01 - 0.2

1 - 50

C S2

G C -FID

CCT

1,2,3 !Trichloropropane

1003


0.01 - 0.2

0.6 - 60

C S2

G C -FID

CCT

T ri c hcylohe xyltin hydrox ide

5504


1 - 1.5

50 - 500


HP LC - G FAAS

GF F & X AD -2

1,1,2 !Tric hlo r o 1,2,2 !trifluoroethane

1020

1,1,2 !TRICHLOR O !1,2,2 ! T R IF L UO R O E T H A N E

0.01 - 0.05

0.1 - 3

C S2

G C -FID

CCT

1,1,2 !Tric hlo r o 1,2,2 !trifluoroethane

2549


0.01 - 0.05

1-6

t h erma l

TD /G C -M S

TD

Triethanolamine

3509


0.5 - 1.0

5 - 300

HSA

IC

IM P

T ri e thyle ne glyc o l

5523

GLYC OLS

0.5 - 2

5 - 60

MeOH

G C -FID

OV S-7

Triethylenetetramine

2540

ETHYLENEDIAMINE, DIETHY LENE TRIAM INE, & T R IE T HY L EN E TE T RA M I N E

0.01 - 0.1

1 - 20

DMF

HP LC - U V

XA D-2 W/1 0% NITC

Trifluorobromomethane

1017


0.01 - 0.05

0.1 - 1

C H 2C l2

G C -FID

2 C C T(lg + sm )

T ri m e llitic anhydride

5036

T R IM E L LI TI C A N HY D R ID E

1.5 - 2

400 - 1000

MeOH

G C -FID

P VC

2,4,7 !Trin it ro flu o re n !9!o n e

5018

2,4,7 !TRINITR O !FLUOREN !9 !O N E

1-3

100 - 500

toluene

HP LC - U V

PTFE

Triortho cre syl ph osp ha te

5037

TRIOR THO CR ESYL P HO SPH ATE

1-3

2 - 100

d ieth y l et h er

GC-FPD

MC EF

Triphe nyl p ho sph ate

5038

TRIPHE NYL P HO SPH ATE

1-3

10 - 400

d ieth y l et h er

GC-FPD

MC EF

T ri phenyltin c hlo r ide

5527

T R IP H E N YL TI N C H L O R ID E

1-4

100 - 2000

TW M

H P LC - IC P

P VC

3/15/2003

MF!23


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Tu be rc le b ac illi

0900

M YC O BA C TER IUM TUB ER C ULO SIS

$4

va r ies

reagent

PCR

PTFE

T ungste n

7301


1-4

50 - 1000

H C l /H N O 3

ICP-AES

MC EF

Tu ng ste n, s olu ble /ins olu ble

7074

TU NGSTEN (sol ubl e/i nso lu b le)

1-4

200 - 1000

H F /H N O 3

FAAS

MC EF

Turpentine

1551

T U RP E N TI N E

0.01 - 0.2

1 - 10

C S2

G C -FID

CCT

Turpentine

2549


0.01 - 0.05

1-6

t h erma l

TD /G C -M S

TD

n-Undecane

1500

HYDROC ARBONS, BP 36-216 oC

0.01 - 0.05

2-2

C S2

G C -FID

CCT

V a ler alde hyde

2018

ALIPHATIC ALDEHYDES

0.1 - 1.5

1 - 15

ACN

HP LC - U V

SG-DNPH

V a ler alde hyde

2536

V A L ER A L D EH Y D E

0.01 - 0.04

0.5 - 10

toluene

G C -FID

X AD -2 /H M P

V a ler alde hyde

2539


0.01 - 0.05

5-5

toluene

G C -F ID /M S

X AD -2 /H M P MC EF

V a nadium

7300


1-4

5 - 2000

H N O 3/HC lO 4

ICP-AES

V a nadium

7301


1-4

5 - 2000

H C l /H N O 3

ICP-AES

MC EF

V a nadium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

V a nadium

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

V a nadium o xide s

7504

VANADIUM OX IDES

1.7 or 2 .2

200 - 1000

T HF

XR D

C Y C & P VC

Viny l ace tate

1453

VINYL A CE TATE

0.1 - 0.2

0.75 - 24

C H 2C l2/M e O H

G C -FID

MS(carbon)

Vinyl benzene

1501


.01 - 1

1 - 14

C S2

G C -FID

CCT

V i nyl br o m ide

1009

V IN Y L B R O M I D E

0.01 - 0.2

2 - 10

Et h a nol

G C !FID

C CT ( lg )

V i nyl c hlor ide

1007

V IN Y L C H L O R ID E

0.05

0.7 - 5

C S2

G C !FID

2 CCT

V i nylide ne c hlo r ide

1015

V IN Y L ID E N E C H LO R I D E

0.01 - 0.2

2.5 - 7

C S2

G C !FID

CCT

V i nylide ne F luo r ide

3800


0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

Vinyl tolueneuene

1501


0.01 - 0.2

1 - 24

C S2

G C !FID

CCT

V M&P naphtha

1550

NAPHTHAS

0.01 - 0.2

1.3 - 20

C S2

G C !FID

CCT

VOCs

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

W ar far in

5002

W AR FA RIN

1-4

200 - 1000

MeOH

HPLC !U V

PTFE

W o o d alc o ho l

2000

M E TH A NO L

0.02 - 0.2

1-5

H 2O/IPA

G C !FID

SG

Xylene

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

X yle ne (o,m ,p )

1501


0.01 - 0.2

2 - 23

C S2

G C !FID

CCT

p -Xylene

3800


0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

m -Xylene

3800


0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

o-Xylene

3800


0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

2,4 !Xylidine

2002


0.02 - 0.2

3 - 20

Et h a nol

G C !FID

SG

Y ttr ium

7300


1-4

5 - 1000

H N O 3/HC lO 4

IC P !AES

MC EF

Y ttr ium

7301


1-4

5 - 1000

H C l /H N O 3

ICP-AES

MC EF

Y ttr ium

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Y ttr ium

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

3/15/2003

MF!24


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max Z in c and c o m po unds

7030

ZINC and compounds, as Zn

1-3

2 - 400

HNO3

FAAS

MC EF

Zinc

7300


1-4

5 - 200

H N O 3/HC lO 4

IC P !AES

MC EF

Zinc

7301


1-4

5 - 200

H C l /H N O 3

ICP-AES

MC EF

Zinc

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

Y ttr ium

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

Z inc o xide

7502

Z IN C O X I D E

1-3

10 - 400

--

XR D

P VC

Z ir c o nium

7300


1-4

5 - 200

H N O 3/HC lO 4

IC P !AES

MC EF

Z ir c o nium

7301


1-4

5 - 200

H C l /H N O 3

ICP-AES

MC EF

Z ir c o nium

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

0500


1-2

7 - 133

NA

G R AV

P VC

0600

PARTICULATES, N.O.R, RESP.

1.7, 2.2 ,2.5

20 - 400

NA

Grav.

CY C & P VC

0800

B IO A E R O S O L SA M P L IN G

28.3

va r ies

NA

va r ies

i m p a c to r

METHODS BY NUM BER

3/15/2003

0801

A ER O BIC B AC TE RIA - G C -F AM E

28.3

50 - 300

hex/MTBE

G C -FID

I m p a c to r

0900

MYCO BACTERIUM TUBERCULOSIS

4

va r ies

reagent

PCR

PTFE

1000

A L LY L C H LO R I D E

0.01 - 1.0

16 - 100

bz

G C !FID

CCT

1001

M E T H YL C H LO R I D E

0.01 - 0.1

0.4 - 3

C H 2C l2

G C !FID

2 C C T (lg + sm )

1002

$!C H L O R O P R E N E

0.01 - 0.1

1.5 - 8

C S2

G C !FID

CCT

1003


0.01 - 0.2

3 - 70

C S2

G C !FID

CCT

1004

DICHLOROETHYL ETHER

0.01 - 1.0

2 - 15

C S2

G C !FID

CCT

1005


0.01 - 0.2

0.5 - 2.5

C S2

G C !FID

2 CCT

1006


0.01 - 0.05

0.3 - 7

C S2

G C !FID

C CT ( lg )

1007

V IN Y L C H L O R ID E

0.05

0.7 - 5

C S2

G C !FID

2 CCT

1008

E T HY L EN E D IB R O M I D E

0.02 - 0.2

0.1 - 25

b z/M e O H

G C !E C D

CCT

1009

V IN Y L B R O M I D E

0.01 - 0.2

2 - 10

Et h a nol

G C !FID

C CT ( lg )

1010

EP ICH LO RO HY DR IN

0.01 - 0.2

2 - 30

C S2

G C !FID

CCT

1011

E T HY L BR O M I D E

0.01 - 0.2

0.5 - 4

IPA

G C !FID

CCT

1012


0.01 - 0.2

2.5 - 10

IPA

G C !FID

2 CCT

1013


0.01 - 0.2

0.1 - 3.5

acet/cyclohexane

G C !E C N

PCT

1014

M E T H YL IO D I D E

0.01 - 1.0

15 - 50

t ol

G C !FID

CCT

1015

V IN Y L ID E N E C H LO R I D E

0.01 - 0.2

2.5 - 7

C S2

G C !FID

CCT

1016


0.01 -0.035

0.5 - 2

C S2

G C !FID

CCT

1017


0.01 - 0.05

0.1 - 1

C H 2C l2

G C -FID

2 C C T(lg + sm )

1018

DICHLORODIFLUORO METHANE, 1,2 !DICHLOROTETR AFLU O R O ! ETHANE& C H L O R O D IF L UO R O M E T H A N E

0.01 - 0.05

1-4

C H 2C l2

G C !FID

2 CCT (lg + sm )

1019


0.01 - 0.2

3 - 30

C S2

G C !FID

PCT

1020

1,1,2 !TRICHLOR O !1,2,2 ! T R IF L UO R O E T H A N E

0.01 - 0.05

0.1 - 3

C S2

G C -FID

CCT

1022

T R IC H L O R O E TH Y L EN E

0.01 - 0.2

1 - 30

C S2

G C -FID

CCT

MF!25


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max

3/15/2003

1024

1,3 !B U TA D IE N E

0.01 - 0.5

5 - 25

C H 2C l2

G C !FID

CCT

1025

1 - a n d 2 -B R O M O P R O P A N E

0.01 - 0.2

0.1 - 12

C S2

G C -FID

CCT

1026

P- C H LO R O B E N Z O T RI FL U O R ID E

0.01 - 0.2

0.1 - 10

C S 2/M e O H

G C -FID

CCT

1300

KETONES I

0.01 - 2.0

1 - 10

C S2

G C !FID

CCT

1301

KE TO NE S II

0.01 - 0.2

1 - 25

M e O H /C S 2

G C !FID

CCT

1302


0.05 - 0.2

0.5 - 125

C H 2C L 2/M e O H

GC-FID/NPD

CCT

1400

ALCOHO LS I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

1401

ALC O HO LS II

0.01 - 0.2

2 - 10

IP A /C S 2

G C !FID

CCT

1402

ALC O HO LS III

0.01 - 0.2

1 - 10

IP A /C S 2

C G !FID

CCT

1403

ALC O HO LS IV

0.01 - 0.05

6 - 50

M e O H /C H 2C l2

G C !FID

CCT

1404

M E TH YL CY C LO H EX AN O L

0.01 - 0.2

1 - 15

C H 2C l2

G C !FID

CCT

1405

ALCOHO LS COM BINED

0.01 - 0.2

2 - 10

IP A -C S 2

G C -FID

CCT

1450

ESTERS I

0.01 - 0.2

1 - 10

C S2

G C !FID

CCT

1451


0.01 - 0.2

0.2 - 20

C S2

G C !FID

CCT

1452

ETHY L FO RM ATE

0.01 - 0.2

0.3 - 10

C S2

G C !FID

CCT

1453

VINYL A CE TATE

0.1 - 0.2

0.75 - 24

C H 2C l2/M e O H

G C -FID

MS(carbon)

1454


0.02 - 0.2

0.1 - 9

C S2

G C !FID

CCT

1457

ETHY L AC ETATE

0.01 - 0.2

0.1 - 10

C S2

G C !FID

CCT

1458

ME THYL A CE TATE

0.01 - 0.2

0.2 - 10

C S2

G C !FID

CCT

1459

ME THYL A CR YLATE

0.01 - 0.2

1-5

C S2

G C !FID

CCT

1460


0.02 - 0.2

0.1 - 9

C S 2/Me th

G C -FID

CCT

1500


0.01 - 0.2

2-7

C S2

G C !FID

CCT

1501


0.01 - 1.0

1 - 30

C S2

G C !FID

CCT

1550

NAPHTHAS

0.01 - 0.2

1.3 - 20

C S2

G C !FID

CCT

1551

T U RP E N TI N E

0.01 - 0.2

1 - 10

C S2

G C -FID

CCT

1552

TERPENES

0.01 - 2

2 - 30

C S2

G C !FID

CCT

1600

C A R B O N D IS U LF ID E

0.01 - 0.2

2 - 25

t ol

G C !FPD

C CT & d ry tu b e

1601

1,1 !DICHLORO !1 !N I TR O E T H AN E

0.01 - 1.0

1.5 - 15

C S2

G C !FID

PCT

1602

D I O X AN E

0.01 - 0.2

0.5 - 15

C S2

G C !FID

CCT

1603

AC ETIC AC ID

0.01 - 0.1

20 - 300

formic a

G C !FID

CCT CCT

1604

AC RYLO NITRILE

0.01 - 0.2

3.5 - 20

a c et/C S 2

G C !FID

1606

AC ETON ITRILE

0.01 - 0.2

1 - 25

C H 2C l2/M e O H

G C !FID

CCT

1608

G LY C ID O L

0.01 - 1.0

5 - 100

T HF

G C !FID

CCT

1609

TETR AHYDR OFU R AN

0.01 - 0.2

1-9

C S2

G C !FID

CCT

1610

ETHYL ETHER

0.01 - 0.2

0.25 - 3

C S2

G C !FID

CCT

1611

METHYLAL

0.01 - 0.2

1-3

hexane

G C !FID

CCT

1612


0.01 - 0.2

0.5 - 5

C S2

G C !FID

CCT

1613

P Y R ID I NE

0.01 - 1.0

18 - 150

C H 2C l2

G C !FID

CCT

1614

E T HY L EN E O X ID E

0.05 - 0.15

1 - 24

DMF

G C !E C D

PC T w/HB r

1615

METH YL tert !BUTYL ETHER

0.1 - 0.2

2 - 96

C S2

G C !FID

2 CC T ( lg )

1616

BUTYL GLYCIDYL ETHER

0.01 - 0.2

15 - 30

C S2

G C !FID

CCT

1617

PHENYL ETHER

0.01 - 0.2

1 - 50

C S2

G C !FID

CCT

MF!26


Chemical

M eth No.


M e th od Na m e

Vol. (L)

E x tr a c ti o n


Sampler

min max

3/15/2003

1618

ISOPROPYL ETHER

0.01 - 0.05

0.1 - 3

C S2

G C !FID

CCT

1619

PHENYL GLYCIDYL ETHER

0.01 - 1

80 - 150

C S2

G C !FID

CCT

1620

ISOPROPYL GLYCIDYL ETHER

0.01 - 0.2

1 - 30

C S2

G C !FID

CCT

2000

M E TH A NO L

0.02 - 0.2

1-5

H 2O/IPA

G C !FID

SG

2002


0.2 - 1.0

30 - 150

Et h a nol

G C !FID

SG

2003


0.2 - 1.0

50 - 100

T HF

G C !FID

SG

2004

DIMETHYLACETAMIDE and D I M E TH Y L FO R M A M I D E

0.01 - 1.0

15 - 80

MeOH

G C !FID

SG

2005


0.01 - 1

1 - 150

MeOH

G C !FID

SG

2007


0.01 - 0.2

4 - 24

M eO H/H 2O

G C !FID

SG

2008

C HLO RO AC ETIC AC ID

0.05 - 0.2

1 - 100

H 2O

IC

SG

2010


0.01 - 1.0

3 - 30

H 2SO 4/a q M e O H

G C !FID

SG

2011

FO RM IC A C ID

0.05 - 0.2

1 - 24

H 2O

IC

P T FE & S G ( w a s h ed )

2012

n !B U TY L AM I N E

0.01 - 1.0

2 - 100

MeOH

G C !FID

S G + H 2SO 4

2013

PHENYL ETHER !DIPHENYL MIXT U R E

0.01 - 0.2

1 - 40

bz

G C !FID

SG

2014

p !C H L O RO P H EN O L

0.05 - 0.2

1.5 - 40

C H 3C N

HPLC !U V

SG

2015

C H L O R O A C E T AL D E HY D E

0.05 - 0.2

3 - 16

MeOH

G C !E C D

SG

2016


0.03 - 1.5

1 - 15

ac eto nitr ile

HP LC - U V

SG/DNPH

2017


0.2

5 - 50

et h a nol

G C -FID

GFF + SG w/H 2SO 4

2018

ALIPHATIC ALDEHYDES

0.1 - 1.5

1 - 15

ACN

HP LC - U V

SG-DNPH

2500


0.01 - 0.2

0.25 - 12

C S2

G C !FID

Carbon be ads

2501

AC RO LEIN

0.01 - 0.1

1.5 - 48

t ol

G C !NPD

X A D !2 /H M P

2504

TETRA ETHY L PYRO PHO SPH ATE

0.01 - 0.2

20 - 48

toluene

G C !FPD

2 Chrom 102

2505

F UR FU RY L A LC O H O L

0.01 - 0.05

3 - 25

a cet

G C !FID

Por Q

2506

AC ETO NE CY AN O HY DR IN

0.2

0.3 - 12

Et Ac

G C !NPD

P or Q S

2507


0.2 - 1.0

3 - 100

Et h a nol

G C !E C D

T e n a x!G C

2508

I SO P H O R O N E

0.01 - 1.0

2 - 25

C S2

G C !FID

PCT

2510

1 !O C TA N ETH IO L

0.01 - 0.2

1 - 15

a cet

G C !FPD

Te na x G C

2513


0.01 - 0.2

2 - 35

IP A /C S 2

G C !FID

PCT

2514

A N IS ID I NE

0.5 - 1.0

24 - 320

MeOH

HPLC !U V

X A D !2

2515

D I AZ O M E T H A N E

0.2

6 - 30

C S2

G C !FID

X A D !2 ( c oa t e d )

2516

D I C H LO R O F L U O R O M E T HA N E

0.01 - 0.05

0.25 - 3

C S2

G C !FID

2 CC T ( lg )

2517

P E N TA C H L O R O E TH A N E

0.01 - 0.2

1 - 10

hexane

G C !E C D

Por R

2518

HEXACHLOR O !1,3 !CYC LO P EN T AD I EN E

0.01 - 0.2

0.25 - 90

hexane

G C !E C D

2 Por T

2519

E T HY L C H LO R I D E

0.02 - 0.05

0.3 - 3

C S2

G C !FID

2 CC T ( lg )

2520

M E T H YL B RO M I D E

0.01 - 0.1

1-5

C S2

G C !AED

PC T(2)+d ry tube

2521

M E T H YL C Y C LO H E X A N O N E

0.01 - 0.05

1-6

a cet

G C !FID

Por Q

2522

NITROSAMINES

0.2 - 2.0

15 - 1000

M e O H /C H 2C l2

G C !TEA

The rma loso rb/N

2523

1,3 !C Y C L O P E N TA D IE N E

0.01 - 0.05

1-5

Et Ac

G C !FID

Chrom104/ ma leic anh .

MF!27


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max

3/15/2003

2524

DIM ETHY L SULFA TE

0.01 - 0.2

0.25 - 12

d iEt eth er

G C !E C N

Por P

2525

n !BU TYL MER CAPTAN

0.01 - 0.05

1-4

a cet

G C !FPD

Chrom 104

2526

N I TR O E T H AN E

0.01 - 0.05

1.5 - 3

Et Ac

G C !FID

2 X A D !2

2527

N I TR O M E T H A N E

0.01 - 0.05

1.2 - 3

Et Ac

G C !FPD

Chrom 106

2528

2 !N I TR O P R O P A N E

0.01 - 0.05

0.1 - 2

Et Ac

G C !FID

Chrom 106

2529

FU R FU R AL

0.01 - 0.05

1 - 12

t ol

G C !FID

X A D !2 /H M P

2530

DIPHENYL

0.01 - 0.5

15 - 30

C C l4

G C !FID

Te na x G C

2532

G L U TA R A LD E H Y D E

0.01 - 0.08

4 - 39

C H 3C N

HPLC !U V

SG/DNPH

2533

TETR AETHYL LEAD (as Pb )

0.01 - 1.0

30 - 200

pentane

G C !PID

X A D !2

2534

TETR AMETHYL LEAD (as P b )

0.01 - 0.2

15 - 100

pentane

G C !PID

X A D !2

2535

T O L UE N E !2,4 !DIISO CY ANA TE

0.2 - 1.0

2 - 170

MeOH

HPLC !U V

GW coated

2536

V A L ER A L D EH Y D E

0.01 - 0.04

0.5 - 10

toluene

G C -FID

X AD -2 /H M P

2537


0.01 - 0.05

1-8

C S2

G C !FID

X A D !2

2538


0.01 - 0.05

1 - 12

t ol

G C !F ID

X A D !2 /H M P

2539


0.01 - 0.05

5-5

t ol

G C !F ID /M S

X A D !2

2540

ETHY LENE DIAM INE, DIETHY LENE TRIAM INE, & T R IE T HY L EN E TE T RA M I N E

0.01 - 0.1

1 - 20

DMF

HPLC !U V

X A D !2 w/10 % N ITC

2541


0.01 - 0.1

1 - 36

t ol

G C !FID

X A D !2 /H M P

2542

M E R C A P TA N S

0.1 - 0.2

10 - 150

H C l/D C E

G C !FPD

GFF/HgAc

2543

H E X A C H LO R O B U T A D IE N E

0.05 - 0.2

1 - 100

hexane

G C !E C D

X A D !2

2544

N I C O TI N E

1.0

60 - 400

Et Ac

G C !NPD

X A D !2

2545

ALLYL GLYCIDYL ETHER

0.01 - 0.2

1.5 - 8

d ieth y l et h er

G C !FID

Tenax

2549


0.01 - 0.05

1-6

t h erma l

TD /G C !M S

TD

2550


1.0 - 2.0

480 - 960

hexane

G C - SC D

PTFE + X D-2

2551

N I C O TI N E

0.1 - 1.0

0.5 - 600

ethy l ace tate

GC-NPD

XA D-4

2552

ME THYL A CR YLATE

0.01 - 0.2

1-5

C S2

G C -FID

A -C M S

2553

KE TO NE S II

0.01 - 0.2

1 - 25

IP A -C S 2

G C -FID

A -C M S

2554

GLYCOL ETHER S

0.1 - 0.2

3 - 25

M e C l2/Me th

G C -FID

A-747

2555

KETONES I

0.01 - 0.2

0.5 - 3.0 1 - 10

C S2

G C -FID

A -C M S

2556

I SO P H O R O N E

0.01 - 1

2 - 25

DEE

G C -FID

XAD

2557

DIACETYL

0.01 - 0.2

1 - 10

Ac et-M eth

G C -FID

A -C M S

2558

AC ETO IN

0.01 - 0.2

1 - 10

Ac et-M eth

G C -FID

A -C M S

2559

D E C A B R O M O D I PH E N Y L O X I D E

2.0

48 - 960

DMSO

HP LC /UV

QFF

2560

1-NITROPYRENE in DIESEL PARTICULATES

1.0 - 2.0

480 - 960

T ol

G C - NC D

GFF

2561

2 -(D IM E TH YL AM IN O )E TH A NO L 1 -D IM E TH YL AM IN O -2 -P RO P AN O L

0.02 - 1

10 - 24

MeOH

G C -FID

XAD

2562

1 , 1, 2 ,2 - TE T RA C H L O R O E TH A N E

0.01 - 0.2

3 - 30

C S2

G C -FID

A -C M S

3500


0.2 - 1.0

1 - 100

NaHSO 3

VIS

P TF E & 2 IM P

3503

H Y D R A ZI N E

0.2 - 1.0

7 - 100

rea ge nts

VIS

BuB

3505

TETRAMETHYL THIOUREA

0.2 - 1.0

50 - 250

rea ge nts

VIS

IMP /H 2O

3506

A C E T IC A N H Y D R ID E

0.2 - 1.0

25 - 100

reagent

VIS

BuB

MF!28


Chemical

M eth No.


M e th od Na m e

Vol. (L)

E x tr a c ti o n


Sampler

min max

3/15/2003

3507


0.1 - 0.5

6 - 60

reagent

HPLC !U V

BuB

3508

M E T H YL E TH Y L K E TO N E P E R O X ID E

0.5 - 0.2

52 - 520

reagent

VIS

IM P

3509


0.5 - 1.0

5 - 300

HSA

IC

IM P

3510

M O N O M E T HY L H YD R A Z IN E

0.5 - 1.5

3 - 20

P M A /H C l

VIS

B u B/H C l

3511

M O N O M E T HY L AN I LI N E

0.2 - 1.0

11 - 100

N a OH

G C !FID

BuB /H 2SO 4

3512

M A L E IC A N H Y D R ID E

0.2 - 1.5

40 - 500

--

HPLC !U V

BuB /H 2O

3513

T E TR A N IT R O M E TH A N E

0.5 - 1.0

20 - 250

!-

G C !FID

I M P /E t A c

3514

E T HY L EN I M IN E

0.2

1 - 48

C H C l3

HPLC !U V

BuB

3515

1,1 !D I M E TH Y L HY D R A Z IN E

0.2 - 1.0

2 - 100

reagent

VIS

Bu B (. 1 M HC l)

3516

C R O T O N A L D EH Y D E

0.1 - 0.2

1 - 49

b u ffer

DPP

BuB

3518

P H E N YL H Y DR A Z IN E

0.2 - 1.0

25 - 120

PMA

VIS

B u B/H C l

3600

MANEB

NA

NA

Cy s/EDTA

HP LC - U V

Patch

3601

MANEB

NA

NA

NA

HP LC - U V

Hand wa sh

3700

B EN ZE NE by po rta ble G C

> 0.02

80% vol

NA

GC

air bag

3701

TR IC H LO R O ETH YL EN E b y p ort G C

> 0.02

80% vol

NA

GC -port

air bag

3702

E TH YL EN E O X ID E b y p orta ble G C

> 0.02

80% vol

NA

G C !PID

air bag

3704

P ER C H LO R O E TH Y LE N E (p o rta b le G C ) in e xh ale d b rea th a nd air

0.1 - 1

8 0% V O L

NA

Po rt G C -PID

air bag

3800


0.1 - 20

Inst r. d ep .

NA

FTIR

Di r. R e a d

4000

TOLU ENE (Diffusive sam pler)

NA

15 min-8h

C S2

G C !FID

Diffusive

5000

C A R BO N B LA C K

1-2

30 - 570

NA

Grav

P VC

5001

2,4 !D an d 2,4,5 !T

1-3

15 - 200

MeOH

HPLC !U V

GFF

5002

W AR FA RIN

1-4

200 - 1000

MeOH

HPLC !U V

PTFE

5003

PARAQUAT

1-4

40 - 1000

H 2O

HPLC !U V

PTFE

5004

H Y D R O Q U IN O N E

1-4

30 - 180

ac etic ac id

HPLC !U V

MC EF

5005

THIRAM

1-4

10 - 400

C H 3C N

HPLC !U V

PTFE

5006

CARBARYL

1-3

20 - 400

reagent

VIS

GFF

5007

ROTENONE

1-4

8 - 400

C H 3C N

HPLC !U V

PTFE

5008

PYRETHUM

1-4

20 - 400

C H 3C N

HPLC !U V

GFF

5009

B E N Z O Y L P E R O X ID E

1-3

40 - 400

d ieth y l et h er

HPLC !U V

MC EF

5010


1-3

2 - 400

C H 3C N

HPLC !U V

PTFE

5011

ETHYLENE THIOUREA

1-3

200 - 800

H 2O

VIS

PVC or MCEF

5012

EPN

1-2

15 - 700

isooctane

G C !FPD

GFF

5013

DYES

1-3

150 - 500

H 2O

HPLC !U V

PTFE

5014

CH LORINA TED TERPH ENYL

1-3

100 - 1500

isooctane

G C !E C D

GFF

5016

S T RY C H N IN E

1-3

70 - 1000

rea ge nts

HPLC !U V

GFF

5017

DIBUTY L PHO SPH ATE

1-3

50 - 250

C H 3C N

G C !FPD

PTFE

5018

2,4,7 !TRINITR O !FLUOREN !9 !O N E

1-3

100 - 500

toluene

HP LC - U V

PTFE

5019

AZ ELA IC A C ID

1-3

200 - 1000

Et h a nol

G C !FID

P VC

5020

D I BU T YL P HT H A LA T E & DI(2 !ETHY LHEX YL) PHTH ALATE

1-3

6 - 200

C S2

G C !FID

MC EF

5021

o !TERPHENYL

1-3

2 - 30

C S2

G C !FID

PTFE

5022

ARSENIC, organo!

1-3

50 - 1000

b u ffer

IC !HYAAS

PTFE

MF!29


Chemical

M eth No.


M e th od Na m e

Vol. (L)

E x tr a c ti o n


Sampler

min max

3/15/2003

5025

C H L O R IN A T ED D IP H E N YL O X ID E

0.5 - 1.5

8 - 200

isooctane

G C !E C N

MC EF

5026

OIL MIST, MINER AL

1-3

20 - 500

C C l4

IR

PVC or MCE

5027

RIB AV IRIN

1-4

5 - 1000

H 2SO 4

HPLC !U V

GFF

5029

4,4'!M E T H YL E N ED I AN I LI N E

1-2

10 - 1000

K O H/M e O H

HPLC !U V

GF F/H 2SO 4

5030

C YA NU RIC AC ID

1-3

10 - 1000

rea ge nts

HPLC !U V

P VC

5031

A SP AR TA M E

1-3

70 - 1200

eluent

HPLC !U V

PTFE

5032

PEN TAM IDINE ISETH ION ATE

1-2

50 - 1500

rea ge nts

HPLC/FL

P VC / o p a q u e

5033

p !N I TR O A N IL IN E

1-3

20

IPA

HPLC !U V

MC EF

5034

TRIBUTY L PHO SPH ATE

1-3

2 - 100

d ieth y l et h er

G C !FPD

MC EF

5035


1-3

50 - 1500

C u (Ac)2

IC P or AAS

P VC

5036

T R IM E L LI TI C A N HY D R ID E

1.5 - 2

400 - 1000

MeOH

G C -FID

P VC

5037

TRIOR THO CR ESYL P HO SPH ATE

1-3

2 - 100

d ieth y l et h er

GC-FPD

MC EF

5038

TRIPHE NYL P HO SPH ATE

1-3

10 - 400

d ieth y l et h er

GC-FPD

MC EF

5039

C H L O R IN A T ED C A M P H E N E

0.2 - 1

2 - 30

p et eth er

G C !E C D

MC EF

5040

ELEMENTAL CARBON (DIESEL PARTICULATE)

2-4

142 -19000

t h erma l

E G A/TO A

QFF

5041


1-3

5 - 1000

C H 3C N

HPLC !FL

GFF

5042


1 -4

28 - 400

benzene

Grav

tared PTFE

5043

p -TO LUE NE SU LFO NIC AC ID

1-3

10 - 1000

1PA /H 20

HP LC - U V

GFF

5044


1

150 - 1000

M eth

HP LC - U V

PTFE

5046

TETRAKIS (HYD RO XYM ETHYL) P H O S P H O N IU M C H L O R ID E

1 - 1.7

1 - 400

ACN

HP LC - U V

GFF

5502

A L D R IN & L IN D A N E

0.2 - 1.0

18 - 240

isooct

G C !E C N

GFF & BuB

5503


0.05 - 0.2

1 - 50

hexane

G C !E C D

G FF & F lor isil

5504


1 - 1.5

50 - 500


HP LC - G FAAS

GF F & X AD -2

5506


2.0

200 - 1000

ac eto nitr ile

HPLC !FL/U V

P T F E & X A D !2

5508

KEPONE

0.5 - 1.0

50 - 600

b z/M e O H

G C !E C D

M C E F & IM P

5509

BENZIDINE and 3,3'!DICHLORO !B E N Z ID I NE

0.2

20 - 100

triethyl amine /M e O H

HPLC !U V

GFF

5510

CHLORDANE

0.5 - 1.0

10 - 200

t ol

G C !E C D


5512

P EN TA C HL OR O PH EN O L

0.5 - 1.0

48 - 480

MeOH

HPLC !U V

MCEF & BuB

5514

D EM E TO N

0.2 - 1.0

30 - 500

t ol

G C !FPD

M C E F & X A D !2

5515


2.0

200 - 1000

va r ies

G C !FID

P T F E & X A D !2

5516

2,4 ! & 2,6 !T O L UE N E D IA M I N E

1.0

30 - 500


HPLC !U V

IM P

5517

POLYCHLORO BENZENES

0.01 - 0.2

3 - 12

hexane

G C !E C D

P T F E & X A D !2

5518

NAPHTHYLAMINES

0.2 - 0.8

30 - 100

acetic a /IPA

G C !FID

GFF & SG

5519

EN DR IN

0.5 - 1.0

12 - 400

t ol

G C !E C D


5521


1.0

5 - 500

rea ge nts

HPLC !EC HD

IM P

5522

ISOCYANATES

1-2

15 - 360

tryptamine/DMSO

HPLC !FL/EC HD

IM P

5523

GLYC OLS

0.5 - 2

5 - 60

MeOH

G C !FID

O VS !7

MF!30


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max

3/15/2003

5524

META LWO RKING FLUIDS (MW F) ALL CATEGO RIES

1.6 - 2.0

1000 - ND

D C M/MeO H/T ol MeOH

Grav

PTFE/CYC

5525


1-2

1 - 500

MAP

HP LC - U V

G F F, IM P

5526

METHYLTIN CHLORIDES

0.25 - 1

15 - 75

AAA

GC-FPD

O VS

5527

T R IP H E N YL TI N C H L O R ID E

1-4

100 - 2000

TW M

H P LC - IC P

P VC

5600


0.2 - 1

12 - 240

t ol/a cet

G C !FPD

O VS !2

5601


0.1 - 1

var - 480

reagent

HP LC - U V

OV S-2

5602


0.2 - 1

12 - 480

reagent

G C /E C D

OV S-2

5603

ALA C HLO R in AIR

1

70 - 1750

MeOH

ELISA

SPE disk

5606

THIO PH EN ATE -M ETH YL in AIR

0.1 - 1.0

20 - 480

IP A /A C N

HP LC - U V

QFF/SST

5700

FORM ALDEHYDE on dust

2

240 - 1050

H 2O /D N PH /C H 3C N

HPLC !U V

I O M / P VC

5701

R ES O RC IN O L

0.2 - 1

5 - 160

MeOH

G C -FID

OV S-7

5800

P O L Y AR O M A T IC C O M P O U N D S (PACs)

1-2

5 - 1000

hexane

FI-FL

PTFE + XA D-2

6001

A R S IN E

0.01 - 0.2

0.1 - 10

HNO3

G FAAS

CCT

6002

P H O S P H IN E

0.01 - 0.2

1 - 16

reagent

6004

S U LF U R D IO X I D E

0.5 - 1.5

4 - 200

H C O 3 /C O 3

-

2-

VIS

S G / H g( C N )2

IC


6005

I O D IN E

0.5 - 1.0

15 - 225

N a 2C O 3

IC

C C T w /alk ali

6006

D I BO R A N E

0.5 - 1.0

60 - 260

H 2O 2

PES

P TF E & C C T w / o xi d iz e r

6007

NICKEL CARBONYL

0.05 - 0.2

7 - 80

HNO3

G FAAS

C C T (lo w N i)

6008

S T IB IN E

0.01 - 0.2

4 - 50

HCl

VIS

S G w /H g C l2

6009

MER CURY

0.15 - 0.25

2 - 100

H N O 3/H C l

AAS !cold va p

Ho pc alite

6010


0.05 - 0.2

2 - 90

H 2O

VIS

s od a lim e

6011


0.3 - 1.0

2 - 90

N a 2S 2O 3

IC

Ag F

6012

S U LF U R Y L F L UO R I D E

0.05 - 0.1

1.3 - 10

N a OH

IC

C CT ( lg )

6013

H Y D R O G E N S UL F ID E (withdrawn)

0.1 - 1.5

1.2 - 40

N H 4OH /H 2O 2

IC

P T FE & C CT ( lg )

6014


0.025

1.5 - 6

reagent

VIS

M S w / T EA & o x id i ze r

6015

AM M O NIA by VIS

0.1 - 0.2

0.1 - 90

H 2O

VIS !Au to

S G + H 2SO 4

6016

AM M O NIA by IC

0.1 - 0.5

0.1 - 96

H 2O

IC

S G + H 2SO 4

6017


0.05 - 2

2 - 90

H 2O

IC -D C Am p

SL

6402

P H O S P H O R U S T R IC H L O R ID E

0.05 - 0.2

11 - 100

rea ge nts

VIS

BuB /H 2O

6600

N I TR O U S O X ID E

NA

80% vol

NA

IR

air bag

6601

OXYG EN

NA

1 - NA

NA

Sens or

po rta ble

6602

S U LF U R H EX A F LU O R ID E

0.01 - 0.05

80% vol

NA

G C !E C D

air bag

6603

C A R B O N D IO X I D E

0.02 - 0.1

80% vol

NA

G C !T C D

air bag

6604

CARBON MONOXIDE

NA

NA

NA

Sens or

Port In str

6700

NITR OGEN DIOX IDE (Di ffu sive)

NA

NA

reagent

VIS

Diffusive

7013

ALUMINUM & CPDS, as Al

1-3

10 - 400

HNO3

FAAS

MC EF

7020

C A LC IU M a nd c pd s a s C a

1-3

20 - 400

H N O 3/HC lO 4

FAAS

MC EF

7024

C H R O M IU M a nd c pd s, as C r

1-3

10 - 1000

H C l /H N O 3

FAAS

MC EF

MF!31


Chemical

M eth No.

M e th od Na m e


Vol. (L)

E x tr a c ti o n


Sampler

min max

3/15/2003

7027

C O B A LT an d c p ds , a s C o

1-3

30 - 1500

a q re g /H N O 3

FAAS

MC EF

7029

CO PPER (dust & fumes)

1-3

50 - 1500

H N O 3/H C l

FAAS

MC EF

7030

ZINC and compounds, as Zn

1-3

2 - 400

HNO3

FAAS

MC EF

7048

C A D M IU M a nd c pd s, as C d

1-3

25 - 1500

H N O 3/H C l

FAAS

MC EF

7056

B A R IU M , S O LU B LE C O M P O U N D S

1-4

50 - 2000

H 2O

FAAS

MC EF

7074

TU NGSTEN (sol ubl e/i nso lu b le)

1-4

200 - 1000

H F /H N O 3

FAAS

MC EF

7082

LEAD by FAAS

1-4

200 - 1500

H N O 3/H 2O 2

FAAS

MC EF

7102

BERYLLIUM and cpds, as Be

1-4

25 - 2000

H N O 3/H 2SO 4

G FAAS

MC EF

7105

LEAD by GFAAS

1-4

1 - 1500

H N O 3/H 2O 2

G FAAS

MC EF

7300


1-4

V a r ies

H N O 3/HC lO 4

IC P !AES

MC EF

7301

E LE M E NT S b y IC P (A Q UA RE G IA AS HIN G )

1-4

V a r ies

Aq R eg

ICP-AES

MC EF PVCF

7301

E LE M E NT S b y IC P (A Q UA RE G IA AS HIN G )

1-4

V a r ies

H C l /H N O 3

ICP-AES

MC EF

7303


1-4

Se e Ta ble

H C l /H N O 3

ICP-AES

MC EF

7400

A S BE ST O S F IB ER S b y PC M

0.5 - 16

400 - va r

NA

PCM

MCEF open

7401

ALKA LINE DU STS

1-4

70 - 1000

HCl

T it ra t ion

PTFE

7402

ASBESTOS FIBERS by TEM

0.5 - 16

400 - va r

NA

TEM

MCEF open

7404

C E LL UL OS E IN SU LA TIO N

1

NA

NA

SEM

ACF

7500

S IL IC A , C R Y ST A LL IN E , b y X R D.

1.7, 2.2 ,2.5

400 - 1000

a s h or T HF

XR D

C Y C + P VC

7501

SILICA, AMOR PHOUS

1.7, 2.2 ,2.5

50 - 400

ash

XR D

PVC (total) PVC&C YC

7502

Z IN C O X I D E

1-3

10 - 400

NA

XR D

P VC

7504

VANADIUM OX IDES

1.7, 2.2 ,2.5

200 - 1000

T HF

XR D

C Y C & P VC

7505

L E AD S U LF ID E

1.7, 2.2 ,2.5

600 - 1000

T HF

XR D

C Y C & P VC

7506

B O R O N C A R B ID E

1.7, 2.2 ,2.5

100 - 1000

ash

XR D

C Y C & P VC

7600


1-4

8 - 400

reagent

VIS

P VC

7601

S IL IC A , C R Y ST A LL IN E

1.7, 2.2 ,2.5

400 - 800

H 3PO 4/HF

VIS

CYC & MC E or P VC

7602

SILICA, CRYSTALLINE (IR )

1.7, 2.2 ,2.5

400 - 800

ash

IR

CYC & MC E or P VC

7603

SILICA in coal mine dust

1.7, 2.2 ,2.5

300 - 1000

ash

IR

C Y C & P VC

7604


1-4

100 - 1000


IC

P VC

7605

CHROM IUM, HEXAV ALEN T b y IONCHROMATOG RAPHY

0.1 - 4

1 - 400

N a O H - N a2C O 3

IC

P VC

7700

LEAD in Air by Che mical Spot Test

2

10 - 240

NA

Sp ot

MC EF

7701

LEAD BY ULTRASOUND /ASV

1-4

20 - 1500

HNO3

Port ASV

MC EF

7702

LEAD by Fi eld Portabl e XR F

1-4

570 - 1900

NA

XR F (po rt)

MC EF

7703

CHROM IUM, HEXAV ALEN T b y Field Portab le Spe ctroph otom etry

1-4

10 - 1200

( N H4) 2SO 4/ N H 4O H

VIS

PVC, MCE, PTFE

7900

AR SENIC & compoun ds , a s As

1-3

30 - 1000

H N O 3/H 2SO 4/HC lO 4

HYAAS

MC EF

7901

AR SENIC TR IOX IDE, as A s

1-3

30 - 1000

H N O 3/H 2O 2

G FAAS

MC EF

7902


1-2

12 - 800

N a OH

ISE


7903


0.2 - 0.5

3.0 - 100

H C O 3-/C O 32-

IC

SG(washed)

MF!32


Chemical

M eth No.


M e th od Na m e

Vol. (L)

E x tr a c ti o n


Sampler

min max

3/15/2003

7904

CYANIDES, aerosol an d g a s

0.5 - 1.0

10 - 180

KOH

ISE

MCEF & BuB

7905

PHOSPHOR U S

0.01 - 0.2

5 - 100

xylene

G C !FPD

Te na x G C

7906

FLU O RID ES by IC

1-2

s 1 - 800 i 120 - 800

N a OH

IC


8301

HIP PU RIC an d M ETH YL H IPP UR IC A C I D in U R IN E

NA

NA

Et a c

HP LC - U V

NA

8315


NA

NA

NA

SC-MSD

Urine

8316

B U TO X Y A C E TI C A C ID in U R IN E

NA

NA

NA

G C - EC D

NA

8317

ANALINE and o-TOLUIDINE in urine

NA

NA

ALK

H P LC - EC D

NA

9000

ASBESTOS, CHRYSOTILE b y XR D

NA

NA

NA

XR D

bu lk

9002

ASBES TOS (bulk) by PLM

NA

NA

NA

PLM

bu lk

9100

LEAD in Surface Wipe Sa mp les

NA

NA

H N O 3/H 2O 2

A A S; IC P

Wipes

9101

CHROM IUM, HEXAV ALENT in s ett led dust

NA

NA

NA

Sp ot

Te st s trip

9102

ELEMENTS on WIPES

NA

NA

NA

ICP-AES

Wipe

9105

LEAD in DUST WIPES by C h emica l Spot Test

NA

NA

NA

Sp ot

Wipe

9200


NA

NA

NA

G C - EC D

polyethylene bag

9201


NA

NA

IPA/diazomethane

G C - EC D

PUF pad

9202

C AP TA N a nd TH IO PH EN AT EM ETH YL in Handrinse

NA

NA

NA

HP LC - U V

Hand wa sh

9205

CAPTAN and THIOPHENATEMETHYL on Dermal Patch

NA

NA

IP A -A C N

HP LC - U V

Patch

MF!33


METHOD FINDER KEY TO ABBREVIATIONS Sampling Media/Devices A-747 Anasorb 747 A-CMS Anasorb CMS Ag F Silver membrane filter BuB Bubbler CCT Coconut shell charcoal tube Chrom Chromosorb CYC Cyclone DNPH Dinitrophenylhydrazine Hcl Dry Drying tube GFF Glass fiber filter GW Glass wool HMP 2! (Hydroxymethyl)piperidine IMP Impinger IOM Inspirable dust sampler MCEF Mixed cellulose ester filter MS Molecular sieve NITC 1! naphthylisothiocyanate OVS! 2 OSHA versatile sampler (quartz filter/XAD! 2) OVS! 7 OSHA versatile sampler ( glass fiber filter/XAD! 7) Pad Cellulose backup pad PCT Petroleum charcoal tube Por Poropak PTFE Polytetrafluoroethylene (Teflon) filter PUF Polyurethane foam PVC Polyvinyl chloride filter QFF Quartz fiber filter SG Silica gel SL Soda lime TD Thermalalal desorption tube TEA Triethanolamine XAD Polymeric resin

Analytical Techniques AAS Atomic absorption spectrophotometry AMP Amperometric detector ASV Anodic stripping voltammetry CD Conductivity detector DPP Differential Pulse Polargraphy ECD Electron capture detector ECHD Electrochemical detector ECN Electrolytic conductivity detector EG Evolved gas analysis FAAS Flame AAS FI Flow injection FID Flame ionization detector FL Fluorescence detector FPD Flame photometric detector GC Gas chromatography Grav Gravimetric (filter weight) GFAAS Graphite furnace AAS HPLC High performance liquid chromatography HYAAS Hydride generation AAS IC Ion chromatography ICP! AES Inductively coupled plasma! atomic emission spectroscopy IR Infrared spoectrophotometry ISE Ion specific electrode MS Mass spectrometry NPD Nitrogen phosphorus detector PCM Phase contrast microscopy PES Plasma emission spectrometry PID Photoionization detector PLM Polarized light microscopy SCD Sulfur chemiluminescence detector SEM Scanning electron microscopy Spot Spot test TCD Thermalalal conductivity detector TEM Transmission electron microscopy TOA Thermal optical analyzer UV Ultraviolet VIS Visible absorption spectrophotometry XRD X! ray diffraction XRF X! ray fluorescence

Extraction Media aaa acetic acid/acetonitrile a acid ac acetate ACN acetonitrile acet acetone al alcohol alk alkali aq aqueous / water aq reg aqua regia bz benzene cychex cyclohexane DCE dichloroethane DMF dimethylformamide DMSO dimethylsulfoxide DNPH dinitrophenyl hydrazine Et ethyl Etac ethyl acetate hex hexane HSA hexanesulfonic acid IPA isopropanol isooct isooctane MeCl2 /Meth methylene chloride/methanol Me methyl Meth methanol MTBE methyl-tert-butyl ether pet petroleum PMA phosphomolybdic acid pyr pyridine reag reagent THF tetrahydrofuran tol toluene TWM tropolone-water-methanol 3/15/2003

Other cap i NA port s var

MF!34

capacity insoluble not applicable portable soluble varies / variable


METHOD FINDER (Key on page MF 34]

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